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[ CAS No. 88597-06-2 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 88597-06-2
Chemical Structure| 88597-06-2
Structure of 88597-06-2 *Storage: {[proInfo.prStorage]}

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Alternatived Products of [ 88597-06-2 ]

Product Details of [ 88597-06-2 ]

CAS No. :88597-06-2MDL No. :MFCD00573287
Formula : C18H17NO5S Boiling Point : -
Linear Structure Formula :-InChI Key :-
M.W :359.40Pubchem ID :-
Synonyms :

Computed Properties of [ 88597-06-2 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 88597-06-2 ]

Signal Word:Class:
Precautionary Statements:UN#:
Hazard Statements:Packing Group:

Application In Synthesis of [ 88597-06-2 ]

  • Downstream synthetic route of [ 88597-06-2 ]

[ 88597-06-2 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 15544-47-5 ]
  • [ 88597-06-2 ]
  • [ 107976-61-4 ]
YieldReaction ConditionsOperation in experiment
99% With caesium carbonate In N,N-dimethyl-formamide for 24h; Ambient temperature;
99% With caesium carbonate In N,N-dimethyl-formamide for 48h; Ambient temperature;
  • 2
  • [ 88597-06-2 ]
  • [ 5457-29-4 ]
YieldReaction ConditionsOperation in experiment
88% With sodium iodide In acetone for 2h; Heating;
78% With tetra-(n-butyl)ammonium iodide In N,N-dimethyl acetamide at 60℃; for 24h; Glovebox; Inert atmosphere; Sealed tube;
With sodium iodide In acetone for 20h; Heating; Yield given;
  • 3
  • [ 15544-47-5 ]
  • [ 88597-06-2 ]
  • [ 107976-61-4 ]
  • [ 107976-59-0 ]
YieldReaction ConditionsOperation in experiment
1: 49% 2: 44% With sodium hydride In N,N-dimethyl-formamide at 85℃;
  • 4
  • [ 883-44-3 ]
  • [ 98-59-9 ]
  • [ 88597-06-2 ]
YieldReaction ConditionsOperation in experiment
96% With triethylamine; In dichloromethane; at 0 - 20℃; for 12.1667h; Step 2To a solution of 2-(3-hydroxypropyl) isoindoline-l,3-dione (1.8 g, 8.77 mmol) in CH2CI2 (30 mL, 3 mL/mmol) was added Et3N (2 mL, 13.1 mmol). After stirring for 10 min at0 C, tosylchloride (2 g, 10.5 mmol) was added and the reaction was stirred for 12 h at RT. The reaction was quenched with water and extracted with CH2CI2 (2 X50 mL). The organic extracts were washed with brine, dried over sodium sulfate and concentrated under reduced pressure. Purification by silica gel column chromatography provided 3-(l,3-dioxoisoindolin-2- yl)propyl 4-methylbenzenesulfonate (3 mg , 96%). Observed mass (M+l): 360.1.
  • 5
  • [ 121821-01-0 ]
  • [ 88597-06-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C 3: benzene / 20 h / 80 °C
  • 6
  • [ 39267-79-3 ]
  • [ 88597-06-2 ]
  • C14H15NO3 [ No CAS ]
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