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[ CAS No. 907212-86-6 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 907212-86-6
Chemical Structure| 907212-86-6
Structure of 907212-86-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 907212-86-6 ]

CAS No. :907212-86-6 MDL No. :MFCD26684656
Formula : C9H4FNO4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 209.13 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 907212-86-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 907212-86-6 ]

[ 907212-86-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2483-57-0 ]
  • [ 347-54-6 ]
  • [ 907212-86-6 ]
YieldReaction ConditionsOperation in experiment
55% With diethyl amine hydrochloride; In toluene;Heating / reflux; [0359] 5-Fluoro-2-hydroxybenzaldehyde (7.14 g, 50.96 mmol), diethyl amine hydrochloride (6.7Og, 61.15 mmol) and <strong>[2483-57-0]methyl nitroacetate</strong> (5.62 mL, 61.15 mmol) were added together in toluene (90 mL) and stirred together at reflux under a N2 atmosphere. A Dean-Stark apparatus was fitted to the system to remove the H2O generated by the reaction. The reaction was allowed to reflux overnight, after which the mixture was cooled and diluted with H2O. The organic layer was separated, washed with brine, dried over anhydrous Na2SO4 and concentrated. Purification by flash chromatography on silica gel afforded the product as an orange solid (5.90 g, 55%)
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