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CAS No. : | 915302-94-2 | MDL No. : | MFCD08690908 |
Formula : | C13H15NO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 233.26 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 6 steps 1: acetyl chloride / 16 h / Heating 2: 80 percent / lithium aluminum hydride / diethyl ether / 3.5 h / Heating 3: 98 percent / thionyl chloride / CHCl3 / 2 h / Heating 4: 60 percent / tricaprylmethylammonium chloride / H2O / 48 h / 100 °C 5: 42 percent / conc. hydrochloric acid / 5 h / Heating 6: H2 / 5percent Pd-C / H2O / 2205.2 Torr |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 6 steps 1: acetyl chloride / 16 h / Heating 2: 85 percent / lithium aluminum hydride / diethyl ether / 3.5 h / Heating 3: 92 percent / thionyl chloride / CHCl3 / 2 h / Heating 4: 67 percent / tricaprylmethylammonium chloride / H2O / 48 h / 100 °C 5: 1.) acetyl chloride, 2.) water / 1.) RT, 48 h, 2.) 1 h 6: 62 percent / H2 / 10percent Pd-C / methanol / 2205.2 Torr |