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[ CAS No. 955365-79-4 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 955365-79-4
Chemical Structure| 955365-79-4
Structure of 955365-79-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 955365-79-4 ]

CAS No. :955365-79-4 MDL No. :
Formula : C23H29NO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 367.48 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 955365-79-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 955365-79-4 ]

[ 955365-79-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 919475-15-3 ]
  • [ 108-94-1 ]
  • [ 955365-79-4 ]
YieldReaction ConditionsOperation in experiment
82% A solution of lithium hexamethyl disilazide (LHMDS) in tetrahydrofuran (388.5ml, 0.46mol) was added to a well stirred solution of acetamide (III) (50g, 0.185mol) in dry tetrahydrofuran (1000ml) maintaining the temperature at -600C to -700C. The mixture was stirred for 15 minutes. Cyclohexanone (23ml, 0.223mol) was added maintaining the temperature at -600C to -700C. After completion of the reaction, a saturated aqueous solution of ammonium chloride was added. Dilute hydrochloric acid was added to adjust <n="14"/>the pH to 4.0 and the mixture was extracted with ethyl acetate (3 x 150ml). The combined organic extracts were washed with water and dried over anhydrous sodium sulphate. Concentration of the extracts afforded the desired amide (IV) as an off-white solid. The structure of the product was confirmed by 1H-NMR. Weight of the product = 56g; molar yield = 82%.
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