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Chemical Structure| 100-96-9 Chemical Structure| 100-96-9

Structure of 100-96-9

Chemical Structure| 100-96-9

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Product Details of [ 100-96-9 ]

CAS No. :100-96-9
Formula : C7H10N2O
M.W : 138.17
SMILES Code : NC1=CC(OC)=CC(N)=C1
MDL No. :MFCD00127692
InChI Key :FLDIDKTWHOYFMG-UHFFFAOYSA-N
Pubchem ID :12897333

Safety of [ 100-96-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P305+P351+P338-P332+P313-P337+P313-P362

Application In Synthesis of [ 100-96-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 100-96-9 ]

[ 100-96-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 74137-36-3 ]
  • [ 100-96-9 ]
YieldReaction ConditionsOperation in experiment
95% With [Cu2(2,7-bis(pyridin-2-yl)-l,8-naphthyridine)(OH)(CF3COO)3]; tetrabutylammomium bromide; ammonia; caesium carbonate; In water; at 120℃; for 16h;Sealed tube; General procedure: A mixture of substrate (0.25 mmol), complex 1 (2.5 × 10? 3 mmol), Cs2CO3 (1 mmol), Conc. NH3(aq) (0.5 mL) and TBAB (0.25 mmol) in water (0.5 mL) were loaded in a sealed reaction tube. The reaction temperature was increased to 110?140 °C and the reaction mixture was stirred for 8?24 h. After cooling to RT, the reaction mixture was poured into a saturated NaCl solution, extracted with ethyl acetate and dried over anhydrous MgSO4. After removal of solvents, the residue was re-crystallized or chromatographed on silica gel. All products were characterized by NMR spectroscopy and were consistent with the literature data.
 

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