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[ CAS No. 101186-77-0 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 101186-77-0
Chemical Structure| 101186-77-0
Structure of 101186-77-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 101186-77-0 ]

CAS No. :101186-77-0 MDL No. :MFCD28975103
Formula : C28H24BrN Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 454.40 Pubchem ID :-
Synonyms :

Safety of [ 101186-77-0 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 101186-77-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 101186-77-0 ]

[ 101186-77-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 101186-77-0 ]
  • [ 156-43-4 ]
  • [ 1554525-40-4 ]
YieldReaction ConditionsOperation in experiment
72.4% With palladium diacetate; sodium t-butanolate; tricyclohexylphosphine In 5,5-dimethyl-1,3-cyclohexadiene; toluene for 3h; Reflux; 1 CTM1 To 100 ml of xylene was added 4.7 g of triphenylamine derivative Compound A, 0.69 g of p-phenetidine, 2.12 g of sodium t-butoxide, 100 mg of palladium acetate,4 ml of a 0.6 mmol / ml toluene solution of tricyclohexylphosphine was introduced, and the temperature was raised until refluxing occurred. After elevated temperature, the mixture was reacted for 3 hours with stirring. After completion of the reaction, the reaction solution was cooled to room temperature, 50 ml of water was added, and the mixture was stirred for 30 minutes. After stirring, the aqueous layer was separated, and the organic layer was concentrated. The concentrated residue was purified by silica gel chromatography to obtain 3.2 g (yield: 72.4%) of a charge transport material CTM1 as a target substance.The IR spectrum of the obtained compound is shown in FIG.
  • 2
  • [ 101186-77-0 ]
  • [ 2708165-32-4 ]
YieldReaction ConditionsOperation in experiment
84% With water-d2; potassium ethyl xanthogenate In N,N-dimethyl-formamide at 150℃; for 24h; Schlenk technique;
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