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[ CAS No. 1023301-73-6 ] {[proInfo.proName]}

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Chemical Structure| 1023301-73-6
Chemical Structure| 1023301-73-6
Structure of 1023301-73-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1023301-73-6 ]

CAS No. :1023301-73-6 MDL No. :MFCD11112288
Formula : C11H22N2O3 Boiling Point : -
Linear Structure Formula :- InChI Key :ODOJNXXZXCRBCC-SECBINFHSA-N
M.W : 230.30 Pubchem ID :51051649
Synonyms :

Safety of [ 1023301-73-6 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1023301-73-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1023301-73-6 ]

[ 1023301-73-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 27996-87-8 ]
  • [ 1023301-73-6 ]
  • (R)-tert-butyl 4-(2-formyl-4-nitrophenyl)-2-(methoxymethyl)piperazine-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
79% With potassium carbonate; In N,N-dimethyl-formamide; at 90℃; for 4h; General procedure: A mixture of 2-chloro-5-nitrobenzaldehyde (2 g, 10.8 mmol), 1-isopropylpiperazine (2.07 g, 16.2 mmol) and potassium carbonate (2.68 g, 19.4 mmol) in DMF (10 mL) was heated at 90 C for 4 h. The reaction mixture wascooled to room temperature and diluted with water. The resulting precipitate was collected by filtration, then washed on the filter with water and dried in a vacuum oven to give the title compound (2.8 g, 96%) . LCMS (Method A) : = 0.49 mi m/z = 278 [M+H].Step 1: (R)-tert-butyl 4-(2-formyl-4-nitrophenyl)-2- (methoxymethyl)piperazine-1-carboxylate<strong>[27996-87-8]2-fluoro-5-nitrobenzaldehyde</strong> (1g. 5.91 mmol) was reactedwith (R)-tert-butyl 2-(methoxymethyl)piperazine-1-carboxylate (1g. 4.34 mmol) following the procedure forexample 21 to give the title compound (1.30 g, 79%)
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