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[ CAS No. 1033811-69-6 ] {[proInfo.proName]}

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Product Details of [ 1033811-69-6 ]

CAS No. :1033811-69-6 MDL No. :MFCD18647943
Formula : C11H12O2 Boiling Point : -
Linear Structure Formula :- InChI Key :LZYXYCODHMBELL-UHFFFAOYSA-N
M.W : 176.21 Pubchem ID :55297325
Synonyms :

Safety of [ 1033811-69-6 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
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Application In Synthesis of [ 1033811-69-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1033811-69-6 ]

[ 1033811-69-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1092553-17-7 ]
  • [ 77-78-1 ]
  • [ 1033811-69-6 ]
YieldReaction ConditionsOperation in experiment
82.5% With potassium carbonate In N,N-dimethyl-formamide at 0 - 65℃; 3.I 3. Preparation of 7-Methoxy-3,6-dimethyl-indan-4-carbaldehyde; Step-I: synthesis of 4-Methoxy-5-methyl-indan-1-one; To a suspension of 4-Hydroxy-5-methyl-indan-1-one (50.0 gm, 0.308 mole) and Potassium carbonate (127.0 gm, 0.928 mole) in Dimethylformamide (250 ml), Dimethyl sulphate (90 ml, 0.928 mole) was added at 0° C. The reaction mixture was heated at 60-65° C. and stirred for 16 hours. The reaction mixture was poured into water (1 litre) and extracted with Ethylacetate (3×250 ml). The organic layer was dried over Sodium sulphate and distilled under vacuum to give 10.0 gm of crude product which was purified by column chromatography using Hexane as a mobile phase. The collected fractions were distilled under vacuum to give 45.0 gm of desired product as a viscous oil.Yield: 82.5%NMR (400 mhz, DMSO-d6): δ 7.30 (1H, d), 7.27 (1H, d), 3.84 (3H, s), 3.12 (2H, t), 2.60-2.63 (2H, m), 2.31 (3H, s).
82.5% With potassium carbonate In N,N-dimethyl-formamide at 0 - 65℃; for 16h; 3.I 3. Preparation of 7-Methoxy-3, 6-dimethyl-indan-4-carbaldehydeStep-I: synthesis of 4-Methoxy-5-methyl-indan-1-one; To a suspension of 4-Hydroxy-5-methyl-indan-1-one (50.0gm ,0.308 mole) and Potassium carbonate (127.0 gm, 0.928 mole) in Dimethylformamide (250 ml), Dimethyl sulphate (90 ml, 0.928 mole) was added at O0C. The reaction mixture was heated at 60-650C and stirred for 16 hours.The reaction mixture was poured into water (1 litre) and extracted with Ethylacetate(3X250 ml).The organic layer was dried over Sodium sulphate and distilled under vaccum to give 10.0 gm of crude product which was purified by column chromatography using Hexane as a mobile phase. The collected fractions were distilled under vaccum to give 45.0 gm of desired product as a viscous oil.Yield :82.5 %NMR(400mhz,DMSO-ds):δ 7.30(1 H,d),7.27(1H,d),3.84(3H,s),3.12(2H,t),2.60-2.63(2H,m),2.31 (3H,s).
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