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[ CAS No. 1056174-56-1 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 1056174-56-1
Chemical Structure| 1056174-56-1
Structure of 1056174-56-1 *Storage: {[proInfo.prStorage]}

Quality Control of [ 1056174-56-1 ]

Purity: {[proInfo.showProBatch.pb_purity]}

Related Doc. of [ 1056174-56-1 ]

SDS

Product Details of [ 1056174-56-1 ]

CAS No. :1056174-56-1MDL No. :MFCD23132059
Formula :C7H8N2O2Boiling Point :-
Linear Structure Formula :-InChI Key :N/A
M.W :152.15Pubchem ID :58629092
Synonyms :

Computed Properties of [ 1056174-56-1 ]

TPSA : 52.1 H-Bond Acceptor Count : 4
XLogP3 : 0.2 H-Bond Donor Count : 0
SP3 : 0.29 Rotatable Bond Count : 2

Safety of [ 1056174-56-1 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P305 P351 P338UN#:N/A
Hazard Statements:H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1056174-56-1 ]

  • Upstream synthesis route of [ 1056174-56-1 ]

[ 1056174-56-1 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 931-63-5 ]
  • [ 75-36-5 ]
  • [ 1056174-56-1 ]
YieldReaction ConditionsOperation in experiment
97% With cetyltrimethylammonim bromide; cetyltrimethylammonium chloride In 1,2-dichloro-ethane at 70℃; for 0.08 h; Microwave irradiation; Micellar solution General procedure: The mixture of anisole(1c, 0.216 mg, 2 mmol) and acetyl chloride (2a, 0.157 mg, 2 mmol) was treated with CTAB/CTAC, (0.001 mol), in dichloroethane and the resulting reaction mixture was heated in a controlled microwave synthesizer (BiotageInitiator+SP Wave model (0.200W at 2.45 GHz, capped at 60W duringsteady state) for 5 min (attains temperature 100 C and 2 bar pressure). The final product (3o) was isolated by absorbing the reaction mixture into silica geland purifying it by column chromatography using ethyl acetate–petroleumether as the eluent.
Reference: [1] Tetrahedron Letters, 2013, vol. 54, # 26, p. 3431 - 3436
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