Alternatived Products of [ 1057641-71-0 ]
Product Details of [ 1057641-71-0 ]
CAS No. : | 1057641-71-0 |
MDL No. : | MFCD23106219 |
Formula : |
C7H11BrO2
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
207.07
|
Pubchem ID : | - |
Synonyms : |
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Safety of [ 1057641-71-0 ]
Application In Synthesis of [ 1057641-71-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1057641-71-0 ]
- 1
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[ 1057641-71-0 ]
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[ 99620-40-3 ]
Yield | Reaction Conditions | Operation in experiment |
33% |
With polyethylene glycol; sodium hydroxide In water; benzene for 12h; Heating / reflux; |
8.b.f
Step f: Preparation of 2-methylidene-5,8-dioxaspiro [3.4] octaneA mixture of 2-(bromomethyl)-5,8-dioxaspiro[3.4]octane (1.3 gm, 6.28 mmol) (step e), polyethylene glycol (PEG-600) (0.5 gm), 50 % aqueous sodium hydroxide solution (5 ml) and benzene was refluxed for about 12 hours. The reaction mixture was cooled, diluted with water and extracted with diethyl ether. The organic layer was washed with brine, dried over sodium sulphate and concentrated under reduced pressure to get a crude product, which was purified by column chromatography.Yield: 0.26 gm (33%) |