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[ CAS No. 1057641-71-0 ] {[proInfo.proName]}

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Chemical Structure| 1057641-71-0
Chemical Structure| 1057641-71-0
Structure of 1057641-71-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1057641-71-0 ]

CAS No. :1057641-71-0 MDL No. :MFCD23106219
Formula : C7H11BrO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 207.07 Pubchem ID :-
Synonyms :

Safety of [ 1057641-71-0 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P270-P301+P312-P330-P501 UN#:
Hazard Statements:H302 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1057641-71-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1057641-71-0 ]

[ 1057641-71-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1057641-71-0 ]
  • [ 99620-40-3 ]
YieldReaction ConditionsOperation in experiment
33% With polyethylene glycol; sodium hydroxide In water; benzene for 12h; Heating / reflux; 8.b.f Step f: Preparation of 2-methylidene-5,8-dioxaspiro [3.4] octaneA mixture of 2-(bromomethyl)-5,8-dioxaspiro[3.4]octane (1.3 gm, 6.28 mmol) (step e), polyethylene glycol (PEG-600) (0.5 gm), 50 % aqueous sodium hydroxide solution (5 ml) and benzene was refluxed for about 12 hours. The reaction mixture was cooled, diluted with water and extracted with diethyl ether. The organic layer was washed with brine, dried over sodium sulphate and concentrated under reduced pressure to get a crude product, which was purified by column chromatography.Yield: 0.26 gm (33%)
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