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Chemical Structure| 1121527-35-2 Chemical Structure| 1121527-35-2

Structure of 1121527-35-2

Chemical Structure| 1121527-35-2

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Product Details of [ 1121527-35-2 ]

CAS No. :1121527-35-2
Formula : C11H21NO4
M.W : 231.29
SMILES Code : O=C(O)CCCN(C(OC(C)(C)C)=O)CC
MDL No. :MFCD23701763
InChI Key :CKXUDWYHHDGVRC-UHFFFAOYSA-N
Pubchem ID :57606003

Safety of [ 1121527-35-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1121527-35-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 1121527-35-2 ]

[ 1121527-35-2 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 76572-84-4 ]
  • [ 24424-99-5 ]
  • [ 1121527-35-2 ]
YieldReaction ConditionsOperation in experiment
76% With potassium carbonate In 1,4-dioxane; water at 23℃; 4-(Ethylamino)butanoic acid (1.15 g, 8.77 mmol) was dissolved in a mixture of dioxane (50 mL) and water (50.0 mL) containing potassium carbonate (0.997 mL, 17.53 mmol) at 0° C. Di-tert-butyl dicarbonate (2.218 mL, 9.64 mmol) was added and the solution was stirred at 23° C. overnight.
The solvent was concentrated.
The aqueous residue was washed with ether.
The aqueous layer was then acidified with 5percent KHSO4 and extracted (2*) with EtOAc.
The organic phase was dried over anhydrous MgSO4 and evaporated. (1.55 g, 76percent).
1H NMR (400 MHz, CHLOROFORM-D) .box. 1.11 (t, J=7.03 Hz, 3H), 1.46 (s, 9H), 1.85 (dt, J=14.06, 7.03 Hz, 2H), 2.37 (t, J=7.03 Hz, 2H), 3.16-3.32 (m, 4H); (M+H)=232.27.
References: [1] Patent: US2009/62251, 2009, A1, . Location in patent: Page/Page column 104.
 

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