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[ CAS No. 115081-94-2 ] {[proInfo.proName]}

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Chemical Structure| 115081-94-2
Chemical Structure| 115081-94-2
Structure of 115081-94-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 115081-94-2 ]

CAS No. :115081-94-2 MDL No. :MFCD11519432
Formula : C8H4INO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 289.03 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 115081-94-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

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[ 115081-94-2 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 115081-94-2 ]
  • [ 144550-76-5 ]
YieldReaction ConditionsOperation in experiment
80% With sodium hydroxide In methanol d.
Methyl 2-amino-4-iodobenzoate
To a stirred solution of sodium hydroxide (0.048 g, 1.2 mM) in methanol (4.5 mL) was added 7-iodo-2H-3,1-benzoxazine-2,4(1H)-dione (2.6 g, 9.0 mM).
The mixture was heated at 60° C. for 7 hr and the resulting solution was cooled, poured into water and extracted with ethyl acetate.
The combined extracts were washed once with dilute sodium hydroxide, dried (MgSO4), filtered and concentrated to leave the title compound (2.0 g, 80percent) as a brown oil which slowly crystallized; MS(CI): 278 (M+H).
Reference: [1] Patent: US5599814, 1997, A,
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