Home Cart Sign in  
Chemical Structure| 1155573-56-0 Chemical Structure| 1155573-56-0

Structure of 1155573-56-0

Chemical Structure| 1155573-56-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1155573-56-0 ]

CAS No. :1155573-56-0
Formula : C10H10BrN3
M.W : 252.11
SMILES Code : NC1=CC(C)=NN1C2=CC=CC=C2Br
MDL No. :MFCD08456848

Safety of [ 1155573-56-0 ]

Application In Synthesis of [ 1155573-56-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1155573-56-0 ]

[ 1155573-56-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1118-61-2 ]
  • [ 16732-66-4 ]
  • [ 1155573-56-0 ]
YieldReaction ConditionsOperation in experiment
76% General procedure: 3-aminocrotononitrile (48, 10 mmol) was added to a suspension of the appropriate arylhydrazine 49a-l (10 mmol) in 12M HCl-H2O (12 mL, 1:3), and the resulting mixture was heated under reflux for 12 hours and then cooled and neutralized with 2.5M sodium hydroxide solution. The suspension was extracted with CH2Cl2 (3x30 mL). The organic phases were washed with brine (20 mL), dried and the solvent evaporated in vacuo. The residue oil was triturated with hexane to obtain a solid which was separated by filtration. Subsequent chromatography was performed where indicated.
 

Historical Records

Technical Information

Categories