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Chemical Structure| 1177423-62-9 Chemical Structure| 1177423-62-9

Structure of 1177423-62-9

Chemical Structure| 1177423-62-9

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Product Details of [ 1177423-62-9 ]

CAS No. :1177423-62-9
Formula : C5H8N4OS
M.W : 172.21
SMILES Code : O=C(C1=NN=C(N)S1)NCC
MDL No. :MFCD23949058

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Application In Synthesis of [ 1177423-62-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1177423-62-9 ]

[ 1177423-62-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 64837-53-2 ]
  • [ 75-04-7 ]
  • [ 1177423-62-9 ]
YieldReaction ConditionsOperation in experiment
In methanol; water; at 20℃; To a suspension of ethyl 5-amino-l,3,4-thiadiazole-2-carboxylate (200 mg, 1.155 mmol) in methanol (1.5 mL) was added a 70percent aqueous solution of ethylamine (0.5 mL, 6.29 mmol). The mixture was stirred at room temperature overnight, concentrated, mixed with water and lyophilized to give 5-amino-N-ethyl- l,3,4-thiadiazole-2-carboxamide as a yellowish solid (200 mg). MS (ES+) m/z: 173 (M+H); LC retention time: 0.70 min (analytical HPLC Method A).
 

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