* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
6-butyl-2-(2',4'-difluorophenyl)-(N-B)-1,3,6,2-dioxazaborocane[ No CAS ]
[ 616-38-6 ]
[ 1190989-12-8 ]
Yield
Reaction Conditions
Operation in experiment
83%
Stage #1: 6-butyl-2-(2',4'-difluorophenyl)-(N-B)-1,3,6,2-dioxazaborocane With lithium diisopropyl amide In tetrahydrofuran at -75℃; for 0.5h;
Stage #2: carbonic acid dimethyl ester In tetrahydrofuran at -75℃; for 0.5h;
Stage #3: With sulfuric acid; water In tetrahydrofuran