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[ CAS No. 1207203-37-9 ] {[proInfo.proName]}

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Chemical Structure| 1207203-37-9
Chemical Structure| 1207203-37-9
Structure of 1207203-37-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1207203-37-9 ]

CAS No. :1207203-37-9 MDL No. :MFCD28501967
Formula : C18H17NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 311.33 Pubchem ID :-
Synonyms :

Safety of [ 1207203-37-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1207203-37-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1207203-37-9 ]

[ 1207203-37-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 757239-60-4 ]
  • [ 1207203-37-9 ]
  • 2
  • [ 1207203-37-9 ]
  • [ 104641-60-3 ]
  • O1-benzyl-O3-[(3R)-1-methylpyrrolidin-3-yl]-3-phenylazetidine-1,3-dicarboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
73% A stirred suspension of 1 -benzyloxycarbonyl-3 -phenyl-azetidine-3 -carboxylic acid (352 mg, 1.04 mmol) in CHC13 (20 mL) 2 drops of DMF were added. The mixture was cooled in an ice-bath and oxalyl chloride (0.14 mL, 1.67 mmol) was added with dropwise. After stirring in the cold bath for a further 10 minutes the mixture was stirred at roomtemperature for 2 hours. The solvent was removed in vacuo, co-evaporated further with CHC13 (20 mL). The residue was taken up with CHC13 (5 mL) and the resulting solution was added dropwise to a solution of (R)- 1 -methylpyrrolidin-3-ol (0.13 mL, 1.15 mmol) in CHC13 (5 mL) at 0 C under N2. The mixture was stirred at 0 C for 30 minutes and allowed to warm to room temperature overnight. The reaction mixture was washed withH20 (2 x 10 mL), the organic phase was separated and the solvent removed in vacuo. The residue was taken up in EtOAc (20 mL) and washed with saturated NaHCO3 solution (2 x 10 mL). The organic phase was separated, filtered through a phase separator and the solvent removed in vacuo to give the title compound as a brown gum (301 mg, 73%). LCMS (Method 1): [MH+] = 395 at 2.69 mm.
  • 3
  • [ 97628-92-7 ]
  • [ 1207203-37-9 ]
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