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[ CAS No. 121269-45-2 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 121269-45-2
Chemical Structure| 121269-45-2
Chemical Structure| 121269-45-2
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Product Details of [ 121269-45-2 ]

CAS No. :121269-45-2 MDL No. :MFCD00269692
Formula : C10H11NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :CMYHFJFAHHKICH-VIFPVBQESA-N
M.W : 177.20 Pubchem ID :11126817
Synonyms :

Safety of [ 121269-45-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 121269-45-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 121269-45-2 ]

[ 121269-45-2 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 24424-99-5 ]
  • [ 121269-45-2 ]
  • [ 119878-90-9 ]
YieldReaction ConditionsOperation in experiment
78% With triethylamine In ethyl acetate for 6h; Ambient temperature;
In ethyl acetate at 25℃; for 16h; Yield given;
  • 2
  • [ 620-72-4 ]
  • [ 56613-80-0 ]
  • [ 121269-45-2 ]
YieldReaction ConditionsOperation in experiment
24% With N-ethyl-N,N-diisopropylamine; In acetonitrile; To a solution of phenylbromoacetate (18.58 g, 86 mmol) in CH3CN under nitrogen was added a solution of (R)-phenylglycinol (10.17 g, 74 mmol) and di-isopropylethylamine (34 ml_, 195 mmol) in CH3CN. The volatiles were removed under reduced pressure keeping the bath temperature below 25 0C to obtain an oil that was treated with EtOAc (120 mL) and stirred for 15 min. The resulting white precipitate was removed by filtration. The filtrate was concentrated under reduced pressure and the desired product was isolated using column chromatography (SiO2) with a step gradient of 10 percent to 50 percent [v/v] EtOAc in cyclohexane to give after evaporation (f?)-5-phenylmorpholin-2- one EBE 06134 (3.17 g, 24 percent yield) as a white solid.MW: 177.2; Yield: 24 percent; White Solid; Mp (0C): 50.3Rf\\ 0.30 (EtOAc:cyclohexane = 50:50). 1H-NMR (CDCI3, delta): 1.99 (s, 1 H, NH), 3.89 (q, 2H, J = 17.8 Hz, N-CH2), 4.18(dd, 1 H, J = 3.7 Hz, J = 10.3 Hz, 0-CH), 4.29 (t, 1 H, J = 10.5 Hz, N-CH), 4.40(dd, 1 H, J = 3.7 Hz, J = 10.5 Hz, 0-CH), 7.30-7.45 (m, 5H, ArH).13C-NMR (CDCI3, delta): 46.8, 54.8, 72.8, 125.3 (2xC), 127.0, 127.3 (2xC), 135.9,166.0. [G]22D = + 30.3 ° (c = 1.00, MeOH).
  • 3
  • [ 2765-11-9 ]
  • [ 121269-45-2 ]
  • (2R,6R,7S,9R)-2-phenyl-7,9-ditetradecyl-1-aza-4,8-dioxabicyclo[4.3.0]nonan-5-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
68% With 4 A molecular sieve In toluene for 120h; Heating;
  • 4
  • [ 629-90-3 ]
  • [ 121269-45-2 ]
  • (2R,6R,7S,9R)-2-phenyl-7,9-dihexadecyl-1-aza-4,8-dioxabicyclo[4.3.0]nonan-5-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
56% With 4 A molecular sieve In toluene for 120h; Heating;
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