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[ CAS No. 1239463-43-4 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 1239463-43-4
Chemical Structure| 1239463-43-4
Structure of 1239463-43-4 *Storage: {[proInfo.prStorage]}

Quality Control of [ 1239463-43-4 ]

Related Doc. of [ 1239463-43-4 ]

SDS
Alternatived Products of [ 1239463-43-4 ]
Alternatived Products of [ 1239463-43-4 ]

Product Details of [ 1239463-43-4 ]

CAS No. :1239463-43-4MDL No. :MFCD20527917
Formula : C9H5BrFN Boiling Point : -
Linear Structure Formula :-InChI Key :N/A
M.W :226.05Pubchem ID :68757738
Synonyms :

Computed Properties of [ 1239463-43-4 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 1239463-43-4 ]

Signal Word:WarningClass:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1239463-43-4 ]

  • Downstream synthetic route of [ 1239463-43-4 ]

[ 1239463-43-4 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 1075-11-2 ]
  • [ 1239463-43-4 ]
YieldReaction ConditionsOperation in experiment
With N-Bromosuccinimide; sulfuric acid; at 0℃; To a stirring mixture of <strong>[1075-11-2]6-fluoroisoquinoline</strong> in H2SO4 (5 mL) at 0 0C was added solid NBS (1.5 EQ) slowly over 5 min. The reaction mixture was reacted at 0 0C for 1 h. To this reaction mixture was added NBS (0.5 EQ). The cold bath was then removed. The reaction mixture was reacted until all the starting material was consumed. To this reaction mixture was neutralized with a cold solution of NaOH (5N) until the pH of this mixture >;10. The white solid was filtered off and dissolved in DCM and washed with a solution of NaOH (IN). The organic layer was dried over MgSO4, filtered, and concentrated under reduced pressure. The crude product was purified via a column to give 5-bromo-<strong>[1075-11-2]6-fluoroisoquinoline</strong>. Retention time (min) = 2.810, method [3], MS(ESI) 226.0 (M+H).
  • 2
  • [ 1239463-43-4 ]
  • [ 1571145-38-4 ]
  • 3
  • [ 1239463-43-4 ]
  • [ 1571145-39-5 ]
  • 4
  • [ 1239463-43-4 ]
  • [ 1571145-40-8 ]
  • 5
  • [ 1239463-43-4 ]
  • [ 1571145-41-9 ]
  • 6
  • [ 1239463-43-4 ]
  • [ 1571145-43-1 ]
  • 7
  • [ 1239463-43-4 ]
  • [ 1571145-44-2 ]
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