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Chemistry
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2-Amino-4-iodobenzamide
Chemistry
Organic Building Blocks
Aryls
Amines Amides Iodides Benzene Compounds

[ CAS No. 1241915-20-7 ] {[proInfo.proName]}

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Chemical Structure| 1241915-20-7
Chemical Structure| 1241915-20-7
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Product Details of [ 1241915-20-7 ]

CAS No. :1241915-20-7 MDL No. :
Formula : C7H7IN2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 262.05 Pubchem ID :-
Synonyms :

Safety of [ 1241915-20-7 ]

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Precautionary Statements: UN#:
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Application In Synthesis of [ 1241915-20-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1241915-20-7 ]

[ 1241915-20-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 20776-54-9 ]
  • [ 1241915-20-7 ]
YieldReaction ConditionsOperation in experiment
52% With ammonia; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; at 20℃;Inert atmosphere; [00313] Step A: To a solution of <strong>[20776-54-9]2-amino-4-iodobenzoic acid</strong> (2.5 g, 9.50 mmol) in DMF (10 mL) at rt under argon were added EDCI (2.18 g, 11.40 mmol), 1 - hydroxybenzotriazole (1.54 g, 11.40 mmol), DIEA (1.98 mL, 11.40 mmol), and ammonia (7.0 N solution in MeOH; 1.90 mL, 13.30 mmol). The dark solution was stirred at rt overnight and diluted with H2O until precipitate formed. The precipitate was separated by filtration, washed with H2O, and dried under high vacuum for several hours to afford 2-amino-4-iodobenzamide as a tan solid (1.3 g, 52%). LC-MS (ESI) m/z 263 (M + H)+.
With DIEA; ammonia; benzotriazol-1-ol; In methanol; N,N-dimethyl-formamide; Step A: To a solution of <strong>[20776-54-9]2-amino-4-iodobenzoic acid</strong> (2.5 g, 9.50 mmol) in DMF (10 mL) at room temperature under argon were added EDCI (2.18 g, 11.40 mmol), 1-hydroxybenzotriazole (1.54 g, 11.40 mmol), DIEA (1.98 mL, 11.40 mmol), and ammonia (7.0 N solution in MeOH, 1.90 mL, 13.30 mmol). The dark solution was stirred at room temperature overnight and diluted with H2O until precipitate formed. The precipitate was separated by filtration, washed with H2O, and dried under high vacuum for several hours to afford 2-amino-4-iodobenzamide as a tan solid (1.3 g, 52%). LC-MS (ESI) m/z 263 (M+H)+.
Reference： [1]Patent: WO2010/99379,2010,A1 .Location in patent: Page/Page column 108
[2]Patent: US2012/53176,2012,A1
[3]Phosphorus, Sulfur and Silicon and the Related Elements,2020,vol. 195,p. 194 - 200

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