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[ CAS No. 1261473-36-2 ]

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2D
Chemical Structure| 1261473-36-2
Chemical Structure| 1261473-36-2
Structure of 1261473-36-2 *Storage: {[proInfo.prStorage]}

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Product Details of [ 1261473-36-2 ]

CAS No. :1261473-36-2MDL No. :MFCD18415687
Formula : C6H5ClFNO Boiling Point : -
Linear Structure Formula :-InChI Key :N/A
M.W :161.56Pubchem ID :-
Synonyms :

Computed Properties of [ 1261473-36-2 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 1261473-36-2 ]

Signal Word:WarningClass:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H320-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1261473-36-2 ]

  • Downstream synthetic route of [ 1261473-36-2 ]

[ 1261473-36-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1369769-03-8 ]
  • [ 74-88-4 ]
  • [ 1261473-36-2 ]
YieldReaction ConditionsOperation in experiment
With silver carbonate; In chloroform; at 40℃; for 5h; (2) 6-chloro-3-fluoro-2-methoxypyridine (325-2)Methyl iodide (262 ul) and silver carbonate (1.12 g) were added to a chloroform (3 ml) solution of the compound 325-1 (300 mg), and the obtained mixture was stirred at 40 C. for 5 hours. The temperature of the reaction solution was cooled to room temperature. The reaction solution was filtered, and the filtrate was concentrated under reduced pressure. The obtained residue was purified by silica gel column chromatography (n-heptane:ethyl acetate=1:0 to 1:1), so as to obtain the title compound (86 mg).1H-NMR (400 MHz, CDCl3) delta (ppm): 4.03 (s, 3H), 6.86 (dd, J=8.0, 2.4 Hz, 1H), 7.30 (dd, J=9.6, 8.0 Hz, 1H)
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