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[ CAS No. 1263060-64-5 ]

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3d Animation Molecule Structure of 1263060-64-5
Chemical Structure| 1263060-64-5
Chemical Structure| 1263060-64-5
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Product Details of [ 1263060-64-5 ]

CAS No. :1263060-64-5 MDL No. :MFCD22038932
Formula : C7H6BrN3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :212.05 Pubchem ID :-
Synonyms :

Safety of [ 1263060-64-5 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1263060-64-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1263060-64-5 ]

[ 1263060-64-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 16461-94-2 ]
  • [ 19125-76-9 ]
  • [ 1263060-64-5 ]
YieldReaction ConditionsOperation in experiment
With acetic acid; In ethanol; at 20℃; for 16h; 3-Amino-4-bromopyrazole (0.331 g, 2.04 mmol) and 3-(dime1hylamino)-2-methyl-2-propenal (0.220 g, 1.94 mmol) were dissolved in acetic acid (6.48 mL) and ethanol (9.72 mL) and the reaction stirred at room temperature for 1 h. Solvents were removed under reduced pressure. The remaining residue was taken up in dichloromethane and purified by column chromatography (20- 80% EtO Ac/Hex) to give the title compound (0.294 g, 1.39 mmol). LRMS (APCI) calc'd for (C7H6BrN3) [M+H , 212.0; found 211.9. 1H NMR (500 MHz, cdcl3) delta 8.44 (s, 2H), 8.04 (s, 1H), 2.40 (s, 3H).
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