Alternatived Products of [ 1263060-64-5 ]
Product Details of [ 1263060-64-5 ]
CAS No. : | 1263060-64-5 |
MDL No. : | MFCD22038932 |
Formula : |
C7H6BrN3
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : | 212.05 |
Pubchem ID : | - |
Synonyms : |
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Safety of [ 1263060-64-5 ]
Application In Synthesis of [ 1263060-64-5 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1263060-64-5 ]
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[ 16461-94-2 ]

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[ 19125-76-9 ]

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[ 1263060-64-5 ]
Yield | Reaction Conditions | Operation in experiment |
|
With acetic acid; In ethanol; at 20℃; for 16h; |
3-Amino-4-bromopyrazole (0.331 g, 2.04 mmol) and 3-(dime1hylamino)-2-methyl-2-propenal (0.220 g, 1.94 mmol) were dissolved in acetic acid (6.48 mL) and ethanol (9.72 mL) and the reaction stirred at room temperature for 1 h. Solvents were removed under reduced pressure. The remaining residue was taken up in dichloromethane and purified by column chromatography (20- 80% EtO Ac/Hex) to give the title compound (0.294 g, 1.39 mmol). LRMS (APCI) calc'd for (C7H6BrN3) [M+H , 212.0; found 211.9. 1H NMR (500 MHz, cdcl3) delta 8.44 (s, 2H), 8.04 (s, 1H), 2.40 (s, 3H). |