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Chemical Structure| 129228-07-5 Chemical Structure| 129228-07-5

Structure of 129228-07-5

Chemical Structure| 129228-07-5

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Product Details of [ 129228-07-5 ]

CAS No. :129228-07-5
Formula : C13H28O2
M.W : 216.36
SMILES Code : COCC(CC(C)C)(CC(C)C)COC
English Name :4,4-Bis(methoxymethyl)-2,6-dimethylheptane
MDL No. :MFCD07780237
InChI Key :PVWCLOAAEFMTLH-UHFFFAOYSA-N
Pubchem ID :21894358

Safety of [ 129228-07-5 ]

Application In Synthesis of [ 129228-07-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 129228-07-5 ]

[ 129228-07-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 129228-07-5 ]
  • [ 886036-77-7 ]
  • [ 7550-45-0 ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
Stage #1: magnesium ethylate; titanium tetrachloride In toluene at 5℃; for 1h; Stage #2: 2,2-di-i-butyl-1,3-dimethoxypropane In toluene at 100℃; for 2h; Stage #3: titanium tetrachloride In toluene at 110℃; for 2h; 76 (Example 76) A polymerization catalyst was prepared and polymerization was carried out in the same manner as in Example 9, except for using 2,2-di(isobutyl)-1,3-dimethoxypropane instead of di-n-butyl phthalate. The results are shown in Table 4.
  • 2
  • [ 74-83-9 ]
  • [ 10547-96-3 ]
  • [ 129228-07-5 ]
YieldReaction ConditionsOperation in experiment
114 g With potassium hydroxide In N,N-dimethyl-formamide at 40 - 60℃; Inert atmosphere; 3.C C. Under the protection of argon, weigh 30g of potassium hydroxide solid, Placed in a 1.0L dry reaction bottle, add N, N- dimethylformamide to dilute potassium hydroxide, make potassium hydroxide mass concentration of 20-30% potassium hydroxide -N, N- dimethylformamide suspension, and then step B prepared a diol solution dropwise added to potassium hydroxide -N, N- dimethylformamide suspension for etherification reaction, diol solution dropwise addition process into the compound e bromomethane gas, control the temperature of the etherification reaction at 40-60 ° C, until the diol solution is dripped to complete, the reaction mixture containing product compound f 3; the reaction mixture 3 is filtered and separated The solids obtained by filtration and separation were washed 2-3 times with n-hexane, the n-hexane wash liquid was collected, the n-hexane wash liquid was mixed with the filtered separated liquid phase, and 114g of the solution containing the compound f isopropyl-2-isoamyl-1,3-dimethoxypropane was obtained by concentrated distillation.
 

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