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Chemical Structure| 129850-61-9 Chemical Structure| 129850-61-9

Structure of 129850-61-9

Chemical Structure| 129850-61-9

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Product Details of [ 129850-61-9 ]

CAS No. :129850-61-9
Formula : C17H33NO4
M.W : 315.45
SMILES Code : CCCCCCCCCCC(NC(OC(C)(C)C)=O)C(O)=O
MDL No. :MFCD08275830

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Application In Synthesis of [ 129850-61-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 129850-61-9 ]

[ 129850-61-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 35237-37-7 ]
  • [ 24424-99-5 ]
  • [ 129850-61-9 ]
YieldReaction ConditionsOperation in experiment
54% Alkaline conditions; 2-Aminododecanoic acid was synthesised as described in the literature with 1-bromodecane and diethyl acetoamidomalonate.26 The free amine of 2-aminohexadecanoic acid was then Boc-protected by reaction with di-tert-butyl dicarbonate in a basic environment as previously reported.26,41 C12 was prepared to afford the pure product in 54.0% yield (1.31g): Rf=0.65 (DCM/MeCN/AcOH); ESI-MS (C17H33NO4, 315.2): m/z=316.4 [M+H]+ (calcd 316.2), 338.2 [M+Na]+ (calcd 338.2); 1H NMR: delta=4.94-4.92 (1H, d, J 7.1Hz, OCONH), 4.26 (1H, m, alpha-CH), 1.82-1.67 (2H, m, beta-CH), 1.42 (9H, s, C(CH3)3), 1.23 (16H, br s, 8CH2), 0.86 (3H, t, J 7.0Hz, CH3).
  • 2
  • [ 73821-97-3 ]
  • [ 129850-61-9 ]
  • [ 47355-10-2 ]
  • HOCOCH2CH2CHNHCOCH(CH2)9CH3NHCOCHNH2(CH2)9CH3CONHCHCH2C8H6NCONH2 [ No CAS ]
  • 3
  • [ 73821-97-3 ]
  • [ 129850-61-9 ]
  • [ 47355-10-2 ]
  • HOCOCH2CH2CHNHCOCH(CH2)9CH3NHCOCHNH2(CH2)2CO2HCONHCHCH2C8H6NCONH2 [ No CAS ]
 

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