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[ CAS No. 1308652-67-6 ] {[proInfo.proName]}

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Chemical Structure| 1308652-67-6
Chemical Structure| 1308652-67-6
Structure of 1308652-67-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1308652-67-6 ]

CAS No. :1308652-67-6 MDL No. :MFCD23702163
Formula : C30H22NP Boiling Point : -
Linear Structure Formula :- InChI Key :JPVSMRIBFLAYKE-UHFFFAOYSA-N
M.W : 427.48 Pubchem ID :118878614
Synonyms :

Safety of [ 1308652-67-6 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1308652-67-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1308652-67-6 ]

[ 1308652-67-6 ] Synthesis Path-Downstream   1~12

  • 2
  • [ 86-74-8 ]
  • [ 1308652-67-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: copper oxide (I); tripotassium phosphate tribasic; N,N-dimethyl-1,2-diaminoethane / toluene / 120 °C 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere 2.2: -78 - 20 °C / Inert atmosphere
Multi-step reaction with 2 steps 1.1: potassium hydroxide / N,N-dimethyl-formamide / 6 h / 155 °C 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere 2.2: 12 h / -78 - 20 °C / Inert atmosphere
Multi-step reaction with 2 steps 1.1: copper (I) iodide; potassium carbonate / 5,5-dimethyl-1,3-cyclohexadiene / 168 h / Inert atmosphere; Reflux 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere 2.2: 12 h / -78 - 20 °C / Inert atmosphere
Multi-step reaction with 2 steps 1.1: N<SUP>1</SUP>,N<SUP>2</SUP>-dimethylethane-1,2-diamine; tripotassium phosphate tribasic; copper oxide (I) / toluene / 72 h / 120 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; isopropanol; propan-2-one / 0.5 h / -78 - 20 °C / Inert atmosphere 2.2: 20 °C / Inert atmosphere

  • 3
  • [ 583-53-9 ]
  • [ 1308652-67-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: copper oxide (I); tripotassium phosphate tribasic; N,N-dimethyl-1,2-diaminoethane / toluene / 120 °C 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere 2.2: -78 - 20 °C / Inert atmosphere
Multi-step reaction with 2 steps 1.1: copper (I) iodide; potassium carbonate / 5,5-dimethyl-1,3-cyclohexadiene / 168 h / Inert atmosphere; Reflux 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere 2.2: 12 h / -78 - 20 °C / Inert atmosphere
Multi-step reaction with 2 steps 1.1: N<SUP>1</SUP>,N<SUP>2</SUP>-dimethylethane-1,2-diamine; tripotassium phosphate tribasic; copper oxide (I) / toluene / 72 h / 120 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; isopropanol; propan-2-one / 0.5 h / -78 - 20 °C / Inert atmosphere 2.2: 20 °C / Inert atmosphere
  • 4
  • [ 1072-85-1 ]
  • [ 1308652-67-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: potassium hydroxide / N,N-dimethyl-formamide / 6 h / 155 °C 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere 2.2: 12 h / -78 - 20 °C / Inert atmosphere
  • 5
  • [ 1308652-67-6 ]
  • [ 160979-17-9 ]
  • [ 2838447-68-8 ]
YieldReaction ConditionsOperation in experiment
70% With bis[chlorido(η2,η2-cycloocta-1,5-diene)rhodium(I)]; Sodium hydrogenocarbonate In toluene at 140℃; for 16h; Schlenk technique; Inert atmosphere;
  • 6
  • [ 141-32-2 ]
  • [ 1308652-67-6 ]
  • [ 2838447-62-2 ]
YieldReaction ConditionsOperation in experiment
87% With bis[chlorido(η2,η2-cycloocta-1,5-diene)rhodium(I)]; Sodium hydrogenocarbonate In toluene at 140℃; for 16h; Schlenk technique; Inert atmosphere;
  • 7
  • [ 1308652-67-6 ]
  • [ 140-88-5 ]
  • [ 2838447-63-3 ]
YieldReaction ConditionsOperation in experiment
86% With silver hexafluoroantimonate; di-μ-chlorobis-[(η6-p-cymene)chlororuthenium(II)]; anhydrous potassium acetate In toluene at 140℃; for 24h; Schlenk technique; Inert atmosphere;
  • 8
  • [ 2495-35-4 ]
  • [ 1308652-67-6 ]
  • [ 2838447-64-4 ]
YieldReaction ConditionsOperation in experiment
85% With bis[chlorido(η2,η2-cycloocta-1,5-diene)rhodium(I)]; Sodium hydrogenocarbonate In toluene at 140℃; for 16h; Schlenk technique; Inert atmosphere;
  • 9
  • [ 2680-03-7 ]
  • [ 1308652-67-6 ]
  • [ 2838447-67-7 ]
YieldReaction ConditionsOperation in experiment
56% With bis[chlorido(η2,η2-cycloocta-1,5-diene)rhodium(I)]; Sodium hydrogenocarbonate In toluene at 140℃; for 16h; Schlenk technique; Inert atmosphere;
  • 10
  • [ 48076-38-6 ]
  • [ 1308652-67-6 ]
  • [ 2838447-65-5 ]
YieldReaction ConditionsOperation in experiment
94% With bis[chlorido(η2,η2-cycloocta-1,5-diene)rhodium(I)]; Sodium hydrogenocarbonate In toluene at 140℃; for 16h; Schlenk technique; Inert atmosphere;
  • 11
  • [ 1308652-67-6 ]
  • [ 4835-96-5 ]
  • [ 2838447-66-6 ]
YieldReaction ConditionsOperation in experiment
89% With bis[chlorido(η2,η2-cycloocta-1,5-diene)rhodium(I)]; Sodium hydrogenocarbonate In toluene at 140℃; for 16h; Schlenk technique; Inert atmosphere;
  • 12
  • [ 1072-85-1 ]
  • [ 86-74-8 ]
  • [ 1308652-67-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: potassium <i>tert</i>-butylate / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere 2.2: 13 h / -78 - 20 °C / Inert atmosphere
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