Alternatived Products of [ 1309982-38-4 ]
Product Details of [ 1309982-38-4 ]
CAS No. : | 1309982-38-4 |
MDL No. : | MFCD09839169 |
Formula : |
C16H24BNO4
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | LJTZQZOLQCVMCV-UHFFFAOYSA-N |
M.W : |
305.18
|
Pubchem ID : | 53398532 |
Synonyms : |
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Safety of [ 1309982-38-4 ]
Application In Synthesis of [ 1309982-38-4 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1309982-38-4 ]
- 1
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[ 263270-02-6 ]
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[ 73183-34-3 ]
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[ 1309982-38-4 ]
Yield | Reaction Conditions | Operation in experiment |
|
With 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate In 1,4-dioxane at 100℃; |
2-6
Reference Example 2-6:[S-ftert-ButoxycarbonvDpyridin-S-yliboronic acidPd(OAc)2 (0.112 g, 0.500 mmol), DPPF (0.554 g, 1.000 mmol), KOAc (1.18 g, 12.0 mmol), tert-butyl 5-bromonicotinate (2.58 g, 10.0 mmol) and bis(pinacolato)diboran (2.79 g, 11.0 mmol) were suspended in 1,4-dioχane (25 ml) and the mixture was stirred at 100°C overnight. The mixture was filtered through celite pad, and the filtrate was evaporated in vacuo. The residue was suspended in acetone (25.0 ml) / H2O (25.0 ml), and sodium periodate (6.41 g,30.0 mmol) and ammonium acetate (2.31 g, 30.0 mmol) were added thereto. The mixture wε. stirred at room temperature for overnight and was diluted with CHCI3 and H2O. The organic layer was washed with H2O, brine, and dried over MgSOφ After flteration and evaporation, the residue was purified by silicagel colunm chromatography (CHCI3 / MeOH) to give intended compound as a brown solid. |