Alternatived Products of [ 1338226-20-2 ]
Product Details of [ 1338226-20-2 ]
CAS No. : | 1338226-20-2 |
MDL No. : | MFCD26402909 |
Formula : |
C11H13N3O2
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | XQKOUEBIJOSTKI-UHFFFAOYSA-N |
M.W : | 219.24 |
Pubchem ID : | 58460055 |
Synonyms : |
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Safety of [ 1338226-20-2 ]
Application In Synthesis of [ 1338226-20-2 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1338226-20-2 ]
- 1
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[ 1338226-20-2 ]

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[ 1182358-83-3 ]
Yield | Reaction Conditions | Operation in experiment |
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With ethanol at 20℃; |
8.b
Step 8(b): 5-(hydroxymethyl)-4-methyl-2,4-dihydro-3H-1,2,4-triazol-3-one (8-3) To a suspension of 5-[(benzyloxy)methyl]-4-methyl-2,4-dihydro-3H-1,2,4-triazol-3-one (8-2; 4.20 g; 19.2 mmol) in EtOH (84 mL) was added Pd(OH)2 (20 wt %; 2.02 g; 2.87 mmol) and the mixture was stirred overnight at room temperature. Filtration through Solka Floe, and in vacuo concentration provided 2.33 g (18.1 mmol; 94%) of the title compound of sufficient purity to be used directly. 1H NMR (500 MHz, DMSO): δ 11.53 (s, 1 H); 5.51 (t, J=5.7 Hz, 1 H); 4.33 (d, J=5.8 Hz, 2 H); 3.17 (s, 3 H). |