Alternatived Products of [ 135774-38-8 ]
Product Details of [ 135774-38-8 ]
CAS No. : | 135774-38-8 |
MDL No. : | MFCD09801456 |
Formula : |
C13H8BrClO
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
295.56
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 135774-38-8 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 135774-38-8 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 135774-38-8 ]
- 1
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[ 289686-74-4 ]
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[ 108-36-1 ]
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[ 135774-38-8 ]
Yield | Reaction Conditions | Operation in experiment |
7% |
Stage #1: 1,3-dibromobenzene With iodine; magnesium In diethyl ether at 20 - 30℃; Inert atmosphere;
Stage #2: 2‐chloro‐N‐methoxy‐N‐methylbenzamide In diethyl ether at 0 - 20℃; Inert atmosphere; |
|
Reference:
[1]Kishore Kumar; Chavarria, Gustavo E.; Charlton-Sevcik, Amanda K.; Arispe, Wara M.; MacDonough, Matthew T.; Strecker, Tracy E.; Chen, Shen-En; Siim, Bronwyn G.; Chaplin, David J.; Trawick, Mary Lynn; Pinney, Kevin G.
[Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 4, p. 1415 - 1419]