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[ CAS No. 1379822-11-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 1379822-11-3
Chemical Structure| 1379822-11-3
Structure of 1379822-11-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1379822-11-3 ]

CAS No. :1379822-11-3 MDL No. :
Formula : C10H4F2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 162.14 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 1379822-11-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1379822-11-3 ]

[ 1379822-11-3 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 28342-75-8 ]
  • [ 1066-54-2 ]
  • [ 1379822-11-3 ]
YieldReaction ConditionsOperation in experiment
<strong>[28342-75-8]1,5-dibromo-2,4-difluorobenzene</strong> (6.4 mmol) was dissolved in ACN (12 mL), and wasadded TEA (2.6 mL), TMS-acetylene (1.6 equiv), CuT (0.16 equiv), and Pd(PPh3)2Cp2 (0.1 equiv) sequentially. The mixture was stirred at 65°C for 6 hours. The mixture was filtered, evaporated and purified on a flash column. The collected fractions were dried and treated with 1 M TBAF in THF for two hours. The solvent was removed on a rotovap. The residue was added EtOAc and water. The organic layer was dried, evaporated and purified on a column.
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