Alternatived Products of [ 1403902-55-5 ]
Product Details of [ 1403902-55-5 ]
CAS No. : | 1403902-55-5 |
MDL No. : | |
Formula : |
C18H27ClN2O2
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
338.87
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 1403902-55-5 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 1403902-55-5 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1403902-55-5 ]
- 1
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[ 1403902-55-5 ]
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[ 1799328-86-1 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 5 steps
1: potassium carbonate; potassium iodide / acetonitrile / 18 h / 70 °C
2: palladium 10% on activated carbon; glacial acetic acid; hydrogen / ethanol / 18 h / 20 °C / 760.05 Torr
3: potassium carbonate; potassium iodide / acetonitrile / 2 h / 20 °C / Cooling with ice
4: hydrogenchloride / 1,4-dioxane; ethyl acetate / 18 h / 20 °C
5: Sodium hydrogenocarbonate / lithium hydroxide monohydrate / 0.33 h / 18.2 °C / pH 7.51 / Inert atmosphere |
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Multi-step reaction with 4 steps
1.1: potassium carbonate; potassium iodide / acetonitrile / 6 h / 15 - 62 °C / Large scale
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 65 - 75 °C / 1500.15 Torr / Large scale
2.2: 1 h / 15 - 25 °C / Large scale
3.1: potassium carbonate; potassium iodide / acetonitrile / 3 h / 15 - 25 °C / Large scale
4.1: hydrogenchloride / 14 h / 0 - 40 °C / Large scale |
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Multi-step reaction with 4 steps
1.1: potassium carbonate; potassium iodide / acetonitrile / 0.9 h / 15 - 62 °C / Large scale
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 65 - 75 °C / 1500.15 Torr / Large scale
2.2: 1 h / 15 - 25 °C / Large scale
3.1: potassium carbonate; potassium iodide / acetonitrile; methanol / 3 h / 15 - 25 °C / Large scale
4.1: hydrogenchloride / 14 h / 0 - 40 °C / Large scale |
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