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Chemical Structure| 1417436-51-1 Chemical Structure| 1417436-51-1

Structure of 1417436-51-1

Chemical Structure| 1417436-51-1

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Product Details of [ 1417436-51-1 ]

CAS No. :1417436-51-1
Formula : C7H14INO
M.W : 255.10
SMILES Code : ICCCN1CCOCC1
MDL No. :MFCD28053458

Safety of [ 1417436-51-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1417436-51-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1417436-51-1 ]

[ 1417436-51-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1417436-51-1 ]
  • C9H6N2O3(2-)*2K(1+) [ No CAS ]
  • [ 199327-61-2 ]
YieldReaction ConditionsOperation in experiment
91.2% With 1-butyl-3-methylimidazolium Tetrafluoroborate; In N,N-dimethyl-formamide; at 75 - 80℃; for 5h; The compound of Formula III dipotassium salt (13.4g, 50mmol) in 40mL DMF was followed by the addition fo 5percent [Bmim]BF4 and the addition of Formula IV (X=I) (15.3g, 60mmol) and was heated to about 75-80°C for 5.0 hours. The reaction mixture was suction filtered to remove the resulting white solid KI. The solvent was distilled DMF and was added with 20mL distilled water. 0.5M hydrochloric acid was added to adjust to pH to 6-7 and stirred at room temperature. The water vapor was distilled off and Formula 1 was obtained (14.6g, 91.2percent yield).
  • 2
  • [ 57616-74-7 ]
  • [ 1417436-51-1 ]
YieldReaction ConditionsOperation in experiment
With sodium iodide; In N,N-dimethyl-formamide; at 60℃; for 3h; A solution of 4(3chloropropy1)niorpholine hydrochloride (Aldrich; 124111g. 062 mrnoi) and sodium iodide (acs. reagent: 0025 mL. 062 mrnoi) inDMF (3. 1 mL) was heated to 60 C for 3 h. The reaction mixture was carried on to the next step as is.
 

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