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Chemistry
Heterocyclic Building Blocks
Pyridines
1-(4-Isopropylpyridin-2-yl)ethanone
Chemistry
Heterocyclic Building Blocks
Organic Building Blocks
Pyridines
Ketones

[ CAS No. 142896-09-1 ]

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3d Animation Molecule Structure of 142896-09-1
Chemical Structure| 142896-09-1
Chemical Structure| 142896-09-1
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Quality Control of [ 142896-09-1 ]

COA NMR CNMR HPLC LC-MS

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SDS
Alternatived Products of [ 142896-09-1 ]

Product Details of [ 142896-09-1 ]

CAS No. :142896-09-1 MDL No. :MFCD17016138
Formula : C10H13NO Boiling Point : -
Linear Structure Formula :- InChI Key :N/A
M.W :163.22 g/mol Pubchem ID :-
Synonyms :

Safety of [ 142896-09-1 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501 UN#:
Hazard Statements:H302-H312-H332 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 142896-09-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 142896-09-1 ]

[ 142896-09-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1122-62-9 ]
  • NH4 S2 O8 [ No CAS ]
  • [ 79-31-2 ]
  • [ 142896-09-1 ]
YieldReaction ConditionsOperation in experiment
5.96 g(30.7%) With silver nitrate In sulfuric acid; water 6 Preparation of 2-acetyl-4-isopropylpyridine (Compound VII) EXAMPLE 6 Preparation of 2-acetyl-4-isopropylpyridine (Compound VII) To a solution of 2-acetylpyridine (11) (14.4 g, 0.12 mol), isobutyric acid (32 g, 0.36 mol) and AgNO3 (4 g, 24 mmol) in 10% H2 SO4 (70 ml) which were heated at 70° C., was added dropwise a solution of NH4 S2 O8 (52 g, 0.23 mmol) in H2 O(120 ml) for 15 min between 70-80° C. After evolution of CO2 ceased, the reaction mixture was stirred at about 80° C. for 15 min and cooled. The solution was washed with ether and the aqueous layer was adjusted at pH 8.0 with sat. K2 CO3 solution and extracted three times with ether/ethyl acetate (1: 1). The organic layer was washed with brine and dried(MgSO4) After removal of the solvent, the residue was chromatographed over silica gel (ether/hexane=3:7) to yield 5.96 g(30.7%) of the comound VII as a colorless oil: IR(film) ν cm-1: 3080, 1700, 1599, 1358, 1202, 843; 1 H--NMR(60MHz, CDCl3) δ 1.25(d, J=7Hz, 6H, two CH3), 2.67(s, 3H, CH3), 2.96(dq, J=7 and 7Hz, 1H, CH), 7.27(dd, J=1.5 and 5Hz, 1H, ArH), 7.87(d, J=1.5Hz, 1H, ArH), 8.50(d, J=5Hz, 1H, ArH);
Reference： [1]Current Patent Assignee: LION CORPORATION; SHIONO KORYO KAISHA LTD - US5214027, 1993, A

Tags: 142896-09-1 synthesis path| 142896-09-1 SDS| 142896-09-1 COA| 142896-09-1 purity| 142896-09-1 application| 142896-09-1 NMR| 142896-09-1 COA| 142896-09-1 structure

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