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[Ti(4-chloro-N-(2,6-dimethylphenyl)-2-hydroxy-5-sulfamoylbenzamide)2(H2O)2]Cl[ No CAS ]
Yield
Reaction Conditions
Operation in experiment
95%
With sodium hydroxide; In acetone; at 20.0℃; for 72.0h;
General procedure: The complexes [Ti(XPD)2(H2O)2]Cl (1), [Ni(XPD)2(H2O)2] (2),[ZrO(XPD)2H2O]·H2O (2), [Pd(XPD)2(H2O)2]·H2O(4), [Ce(XPD)2SO4] (5), and [UO2(XPD)2]·3H2O (6) were synthesized as follows: 0.5 mmol of the corresponding metal salt, TiCl3, NiSO4·6H2O, ZrOCl2·8H2O, PdCl2, Ce(SO4)2, or UO2(NO3)2·6H2O, was dissolved in 20 mL of bidistilled water and added to 1mmol (0.35 g) of XPD and 1 mmol (0.40 g) of NaOHin 25 mL of acetone. The mixture was stirred at room temperature for 3 days, and then left for slow evaporation. The formed precipitates were filtered off, washed several times with bidistilled water, and dried over CaCl2 in a desiccator under vacuum.
[Ni(4-chloro-N-(2,6-dimethylphenyl)-2-hydroxy-5-sulfamoylbenzamide)2(H2O)2][ No CAS ]
Yield
Reaction Conditions
Operation in experiment
76%
With sodium hydroxide; In water; acetone; at 20.0℃; for 72.0h;
General procedure: The complexes [Ti(XPD)2(H2O)2]Cl (1), [Ni(XPD)2(H2O)2] (2),[ZrO(XPD)2H2O]·H2O (2), [Pd(XPD)2(H2O)2]·H2O(4), [Ce(XPD)2SO4] (5), and [UO2(XPD)2]·3H2O (6) were synthesized as follows: 0.5 mmol of the corresponding metal salt, TiCl3, NiSO4·6H2O, ZrOCl2·8H2O, PdCl2, Ce(SO4)2, or UO2(NO3)2·6H2O, was dissolved in 20 mL of bidistilled water and added to 1mmol (0.35 g) of XPD and 1 mmol (0.40 g) of NaOHin 25 mL of acetone. The mixture was stirred at room temperature for 3 days, and then left for slow evaporation. The formed precipitates were filtered off, washed several times with bidistilled water, and dried over CaCl2 in a desiccator under vacuum.
[ZrO(4-chloro-N-(2,6-dimethylphenyl)-2-hydroxy-5-sulfamoylbenzamide)2H2O]*H2O[ No CAS ]
Yield
Reaction Conditions
Operation in experiment
80%
With sodium hydroxide; In water; acetone; at 20.0℃; for 72.0h;
General procedure: The complexes [Ti(XPD)2(H2O)2]Cl (1), [Ni(XPD)2(H2O)2] (2),[ZrO(XPD)2H2O]·H2O (2), [Pd(XPD)2(H2O)2]·H2O(4), [Ce(XPD)2SO4] (5), and [UO2(XPD)2]·3H2O (6) were synthesized as follows: 0.5 mmol of the corresponding metal salt, TiCl3, NiSO4·6H2O, ZrOCl2·8H2O, PdCl2, Ce(SO4)2, or UO2(NO3)2·6H2O, was dissolved in 20 mL of bidistilled water and added to 1mmol (0.35 g) of XPD and 1 mmol (0.40 g) of NaOHin 25 mL of acetone. The mixture was stirred at room temperature for 3 days, and then left for slow evaporation. The formed precipitates were filtered off, washed several times with bidistilled water, and dried over CaCl2 in a desiccator under vacuum.
[Pd(4-chloro-N-(2,6-dimethylphenyl)-2-hydroxy-5-sulfamoylbenzamide)2]*(H2O)2[ No CAS ]
Yield
Reaction Conditions
Operation in experiment
94%
With sodium hydroxide; In acetone; at 20.0℃; for 72.0h;
General procedure: The complexes [Ti(XPD)2(H2O)2]Cl (1), [Ni(XPD)2(H2O)2] (2),[ZrO(XPD)2H2O]·H2O (2), [Pd(XPD)2(H2O)2]·H2O(4), [Ce(XPD)2SO4] (5), and [UO2(XPD)2]·3H2O (6) were synthesized as follows: 0.5 mmol of the corresponding metal salt, TiCl3, NiSO4·6H2O, ZrOCl2·8H2O, PdCl2, Ce(SO4)2, or UO2(NO3)2·6H2O, was dissolved in 20 mL of bidistilled water and added to 1mmol (0.35 g) of XPD and 1 mmol (0.40 g) of NaOHin 25 mL of acetone. The mixture was stirred at room temperature for 3 days, and then left for slow evaporation. The formed precipitates were filtered off, washed several times with bidistilled water, and dried over CaCl2 in a desiccator under vacuum.
[Ce(4-chloro-N-(2,6-dimethylphenyl)-2-hydroxy-5-sulfamoylbenzamide)2SO4][ No CAS ]
Yield
Reaction Conditions
Operation in experiment
79%
With sodium hydroxide; In water; acetone; at 20.0℃; for 72.0h;
General procedure: The complexes [Ti(XPD)2(H2O)2]Cl (1), [Ni(XPD)2(H2O)2] (2),[ZrO(XPD)2H2O]·H2O (2), [Pd(XPD)2(H2O)2]·H2O(4), [Ce(XPD)2SO4] (5), and [UO2(XPD)2]·3H2O (6) were synthesized as follows: 0.5 mmol of the corresponding metal salt, TiCl3, NiSO4·6H2O, ZrOCl2·8H2O, PdCl2, Ce(SO4)2, or UO2(NO3)2·6H2O, was dissolved in 20 mL of bidistilled water and added to 1mmol (0.35 g) of XPD and 1 mmol (0.40 g) of NaOHin 25 mL of acetone. The mixture was stirred at room temperature for 3 days, and then left for slow evaporation. The formed precipitates were filtered off, washed several times with bidistilled water, and dried over CaCl2 in a desiccator under vacuum.
[UO2(4-chloro-N-(2,6-dimethylphenyl)-2-hydroxy-5-sulfamoylbenzamide)2]*3H2O[ No CAS ]
Yield
Reaction Conditions
Operation in experiment
98%
With sodium hydroxide; In water; acetone; at 20.0℃; for 72.0h;
General procedure: The complexes [Ti(XPD)2(H2O)2]Cl (1), [Ni(XPD)2(H2O)2] (2),[ZrO(XPD)2H2O]·H2O (2), [Pd(XPD)2(H2O)2]·H2O(4), [Ce(XPD)2SO4] (5), and [UO2(XPD)2]·3H2O (6) were synthesized as follows: 0.5 mmol of the corresponding metal salt, TiCl3, NiSO4·6H2O, ZrOCl2·8H2O, PdCl2, Ce(SO4)2, or UO2(NO3)2·6H2O, was dissolved in 20 mL of bidistilled water and added to 1mmol (0.35 g) of XPD and 1 mmol (0.40 g) of NaOHin 25 mL of acetone. The mixture was stirred at room temperature for 3 days, and then left for slow evaporation. The formed precipitates were filtered off, washed several times with bidistilled water, and dried over CaCl2 in a desiccator under vacuum.
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