There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 144-48-9 | MDL No. : | MFCD00008028 |
Formula : | C2H4INO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | PGLTVOMIXTUURA-UHFFFAOYSA-N |
M.W : | 184.96 | Pubchem ID : | 3727 |
Synonyms : |
|
Signal Word: | Danger | Class: | 6.1 |
Precautionary Statements: | P261-P280-P301+P310-P342+P311 | UN#: | 2811 |
Hazard Statements: | H301-H317-H334 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
90% | 1.0 g of 6-chlorosalicylaldehyde 9 is dissolved in 30 ml of DMF, 0.26 g of NaH (60percent suspension in paraffin oil) is carefully added with cooling, and the mixture is stirred at RT for 45 min. 1.30 g of 2-iodoacetamide 2 are then added, and the reaction mixture is stirred overnight. The mixture is subsequently subjected to conventional work-up, giving 1.28 g (90percent) of 2-(3-chloro-2-formylphenoxy)acetamide 10 ; MS-EI (M+)=213 |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
54% | With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20℃; | To a mixture of <strong>[97817-23-7]4,5,6,7-tetrahydro[1,3]thiazolo[5,4-c]pyridin-2-amine</strong> (50 mg, 0.322 mmol) and DIPEA (0.072 mL, 0.418 mmol) in THE (3 mL), 2-iodoacetamide (65 mg, 0.354 mmol) was added and the reaction let under stirring at rt overnight. After solvent removal under reduced pressure, the title compound was isolated by column chromatography (eluant DCM:MeOH = 90:10) as white solid (37 mg, 54%).NMR (500 MHz, DMSO-d6) ppm 2.73 (t, J=5.72 Hz, 2 H) 3.03 (s, 2 H) 3.46 (s, 2 H) 6.70 (br. s., 2 H) 7.12 (br. s.,H) 7.23 (br. s., 1 H).HRMS (ESI+): calcd. for 08H13N40S [M + H] 213.0805; found 213.0799. |