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Quality Control of [ 1442461-73-5 ] Purity: 98% SDS Specification

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Product Details of [ 1442461-73-5 ]

CAS No. :	1442461-73-5
Formula :	C₁₆H₁₇BO₆
M.W :	316.11
SMILES Code :	O=C(C1=CC2=CC=C(B3OC(C)(C)C(C)(C)O3)C=C2OC1=O)O
English Name :	2-Oxo-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2H-chromene-3-carboxylic acid
MDL No. :	MFCD34186898
InChI Key :	ROYLDHSKPCMDCZ-UHFFFAOYSA-N
Pubchem ID :	139269705

Safety of [ 1442461-73-5 ]

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Application In Synthesis of [ 1442461-73-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 1442461-73-5 ]

[ 1442461-73-5 ] Synthesis Path-Downstream 1~10

1
[ 105837-04-5 ]
[ 1442461-73-5 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 4 steps 1: sodium hydroxide / methanol; water / 24 h / 20 °C 2: boron trifluoride diethyl etherate 3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 12 h / Schlenk technique; Inert atmosphere; Heating 4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
	Multi-step reaction with 4 steps 1: sodium hydroxide / methanol; water / 24 h / 20 °C 2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap 3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 12 h / Schlenk technique; Inert atmosphere; Heating 4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
	Multi-step reaction with 5 steps 1: sodium hydroxide / methanol; water / 24 h / 20 °C 2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / Inert atmosphere; Cooling with ice 3: triethylamine / dichloromethane / 3.67 h / 0 - 20 °C 4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 12 h / Schlenk technique; Inert atmosphere; Heating 5: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

References: [1]Szijjarto, Csongor; Pershagen, Elias; Ilchenko, Nadia O.; Borbas, K. Eszter [Chemistry - A European Journal, 2013, vol. 19, # 9, p. 3100 - 3109].
[2]Szijjarto, Csongor; Pershagen, Elias; Ilchenko, Nadia O.; Borbas, K. Eszter [Chemistry - A European Journal, 2013, vol. 19, # 9, p. 3100 - 3109].
[3]Szijjarto, Csongor; Pershagen, Elias; Ilchenko, Nadia O.; Borbas, K. Eszter [Chemistry - A European Journal, 2013, vol. 19, # 9, p. 3100 - 3109].

2
[ 1438410-03-7 ]
[ 1442461-73-5 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 3 steps 1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap 2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 12 h / Schlenk technique; Inert atmosphere; Heating 3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
	Multi-step reaction with 3 steps 1: boron trifluoride diethyl etherate 2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 12 h / Schlenk technique; Inert atmosphere; Heating 3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
	Multi-step reaction with 4 steps 1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / Inert atmosphere; Cooling with ice 2: triethylamine / dichloromethane / 3.67 h / 0 - 20 °C 3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 12 h / Schlenk technique; Inert atmosphere; Heating 4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3
[ 1442461-71-3 ]
[ 1442461-73-5 ]