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CAS No. : | 14468-40-7 | MDL No. : | MFCD00065209 |
Formula : | C8H4F3NS | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 203.18 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In hexane; at 25℃; for 0.5h;Mechanism; | In a glove box, to a mixture of <strong>[1295-35-8]Ni(cod)2</strong> (27.5 mg, 0.1 mmol; 1.0 equiv) and IPr (38.9 mg,0.1 mmol; 1.0 equiv) in hexane (0.5 mL) was added 2-trifluoromethylbenzothiazole (20.3mg, 0.1 mmol). The immediately formed precipitate was collected by filtration after 30 minutes, and washed with hexane (3 x 3 mL). From 1H and 13C analyses, the obtainedcomplex was analytically pure. A good crystal suitable for the X-ray analysis wasobtained by the recrystallization from toluene at -30 C. |