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[ CAS No. 14920-87-7 ] {[proInfo.proName]}

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Chemical Structure| 14920-87-7
Chemical Structure| 14920-87-7
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Product Details of [ 14920-87-7 ]

CAS No. :14920-87-7 MDL No. :MFCD01313701
Formula : C8H6Cl2O2 Boiling Point : -
Linear Structure Formula :- InChI Key :HEYGSGDIWJDORA-UHFFFAOYSA-N
M.W :205.03 Pubchem ID :599542
Synonyms :
Methyl 2,6-dichlorobenzoate

Safety of [ 14920-87-7 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 14920-87-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 14920-87-7 ]
  • Downstream synthetic route of [ 14920-87-7 ]

[ 14920-87-7 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 14920-87-7 ]
  • [ 15258-73-8 ]
YieldReaction ConditionsOperation in experiment
95% With zinc(II) tetrahydroborate In ethanol at 78℃; for 3 h; Add 100 ml of absolute ethanol to the four-necked flask and heat to reflux.15 g of the raw material methyl 2,6-dichlorobenzoate was added to the ethanol.10 g of zinc borohydride was slowly added thereto, and the reaction was stirred at 78 ° C for 3 h.After the GC reaction was completed, the solvent was evaporated to dryness to obtain 12 g.2,6-dichlorobenzyl alcohol.The product yield was 95percent and the purity was 98percent.
Reference: [1] Patent: CN108794297, 2018, A, . Location in patent: Paragraph 0007; 0008; 0009
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