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Chemical Structure| 15205-57-9 Chemical Structure| 15205-57-9

Structure of 15205-57-9

Chemical Structure| 15205-57-9

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Product Details of [ 15205-57-9 ]

CAS No. :15205-57-9
Formula : C21H21O3P
M.W : 352.36
SMILES Code : P(OCC1=CC=CC=C1)(OCC2=CC=CC=C2)OCC3=CC=CC=C3
English Name :Tribenzyl phosphite
MDL No. :MFCD19440712

Safety of [ 15205-57-9 ]

Application In Synthesis of [ 15205-57-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15205-57-9 ]

[ 15205-57-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 15205-57-9 ]
  • [ 1707-92-2 ]
YieldReaction ConditionsOperation in experiment
With air
  • 3
  • [ 31251-41-9 ]
  • [ 15205-57-9 ]
  • [ 2170529-72-1 ]
YieldReaction ConditionsOperation in experiment
60% With boron trifluoride diethyl etherate In 1,4-dioxane at 20℃; for 12h; 4 Example 4 Preparation of dibenzyl (8-chloro-6,11 -dihydro-5H-benzo [5,6] cyclohepta [1,2-b] pyridin-11-yl) phosphonate (Id) Tricyclic ketone (4) (10.0 mmol), 1,4-dioxane (20.0 ml) and P (OCH2Ph) 3 (15.0 mmol) were added to the reaction flask,Stir well, add BF3 ether (10.0 mmol) and stir at room temperature for 12 h.After the reaction was completed, methylene chloride (50.0 ml) was added and the reaction was washed with deionized water (30 ml), 10% aqueous sodium carbonate (30 ml) and saturated aqueous NaCl (30 ml), and the organic layer was washed with anhydrous Na2SO4 Drying, filtration, evaporation of the solvent under reduced pressure, purification of the residue by column chromatography on silica gel,Had a pale yellow product, yield 60.0%
 

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