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[ CAS No. 1529801-55-5 ]

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Chemical Structure| 1529801-55-5
Chemical Structure| 1529801-55-5
Structure of 1529801-55-5 * Storage: {[proInfo.prStorage]}

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Alternatived Products of [ 1529801-55-5 ]
Alternatived Products of [ 1529801-55-5 ]

Product Details of [ 1529801-55-5 ]

CAS No. :1529801-55-5 MDL No. :
Formula : C9H4ClF3N2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :232.59 g/mol Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 1529801-55-5 ]

  • Downstream synthetic route of [ 1529801-55-5 ]

[ 1529801-55-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 924-44-7 ]
  • [ 360-60-1 ]
  • [ 1529801-55-5 ]
YieldReaction ConditionsOperation in experiment
35% 3-(Trifluoromethyl)benzene-I,2-diamine (4.4 g, 25 mmol) and ethyl2-oxoacetate (2.7 g, 27mmol) were refluxed in ethanol (50 mL) overnight. The mixture was cooled and the precipitate wascollected by filtration. The precipitate was refluxed overnight in phosphorus oxychloride (30 mL),and then the reaction mixture was concentrated. A solution of sodium hydroxide in water (0.5 M, 20mL) was added, and the reaction mixture was extracted with chloroform. The crude product was25 purified by silica gel column chromatography eluting with chloroform to afford I.4 g, 35percent of thetitled compound as a brown solid. MS (ESI) m/z 233.4 (M+ It.
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