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[ CAS No. 1568026-19-6 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
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3d Animation Molecule Structure of 1568026-19-6
Chemical Structure| 1568026-19-6
Chemical Structure| 1568026-19-6
Structure of 1568026-19-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1568026-19-6 ]

CAS No. :1568026-19-6 MDL No. :MFCD21645752
Formula : C6H11F2NO Boiling Point : -
Linear Structure Formula :- InChI Key :GLSFKVZLDBCSSQ-YFKPBYRVSA-N
M.W : 151.15 Pubchem ID :64115141
Synonyms :

Safety of [ 1568026-19-6 ]

Signal Word:Danger Class:8
Precautionary Statements:P210-P261-P264-P270-P271-P280-P302+P352-P304+P340-P305+P351+P338-P310-P330-P332+P313-P362-P370+P378-P403+P233-P403+P235-P405-P501 UN#:1760
Hazard Statements:H302-H315-H318-H335-H227 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1568026-19-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1568026-19-6 ]

[ 1568026-19-6 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 1568026-19-6 ]
  • [ 845936-94-9 ]
  • [ 2351140-24-2 ]
YieldReaction ConditionsOperation in experiment
54% Stage #1: (S)-1-(2,2-difluoroethyl)pyrrolidin-3-ol; 2-(7-hydroxy-9H-thioxanthen-4-yl)-6-morpholino-4H-pyran-4-one With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 71h; Inert atmosphere; Stage #2: With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; N,N-dimethyl-formamide at 60 - 70℃; for 40h; Inert atmosphere;
  • 2
  • [ 1568026-19-6 ]
  • [ 124-63-0 ]
  • [ 2766070-71-5 ]
YieldReaction ConditionsOperation in experiment
260 mg With triethylamine In dichloromethane at 20℃; for 1.5h; Intermediate 204: (S)-1-(2,2-difluoroethyl)pyrrolidin-3-yl methanesulfonate Intermediate 204 was isolated as a beige solid (260 mg) according to general procedure 5f, starting from (S)-1-(2,2-difluoroethyl)pyrrolidin-3-ol (100 mg, 0.63 mmol). M/Z (M+H)+: 230.0. General Procedure 5f: electrophile formation - mesylation To a solution of an alcohol (1.0 equiv) in DCM (0.2 M) was added triethylamine (1.1 equiv) and methanesulfonyl chloride (1.1 equiv). The reaction mixture was stirred at rt for 1 h. In case of uncomplete conversion, triethylamine (0.5 equiv) and methanesulfonyl chloride (0.5 equiv) were added and the reaction mixture was stirred at rt for 30 min. The mixture was concentrated to dryness and co-evaporated twice with toluene. The product was further purified when necessary.
  • 3
  • [ 1568026-19-6 ]
  • [ 2766067-01-8 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: triethylamine / dichloromethane / 1.5 h / 20 °C 2.1: sodium hydride / tetrahydrofuran; mineral oil 2.2: 19 h / 70 °C
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