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Chemical Structure| 17059-52-8 Chemical Structure| 17059-52-8

Structure of 17059-52-8

Chemical Structure| 17059-52-8

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Product Details of [ 17059-52-8 ]

CAS No. :17059-52-8
Formula : C9H8O
M.W : 132.16
SMILES Code : CC1=C(OC=C2)C2=CC=C1
MDL No. :MFCD00138125

Safety of [ 17059-52-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H227-H315-H319-H335
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 17059-52-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17059-52-8 ]

[ 17059-52-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 110-00-9 ]
  • [ 534-22-5 ]
  • [ 271-89-6 ]
  • [ 17059-52-8 ]
  • [ 5670-23-5 ]
  • [ 59020-74-5 ]
  • [ 4265-25-2 ]
YieldReaction ConditionsOperation in experiment
2.8%; 1.9%; 2.7% With aluminum (III) chloride; acetic acid; In water; at 140℃; for 3h; Preparing an aqueous acetic acid solution having a volume ratio of acetic acid to water of 3:1,2 mL of this aqueous acetic acid solution was added to a 10 ml reaction tube, and 0.01 g of furan, 0.01 g of 2-methylfuran and 0.1 g of an aluminum chloride catalyst were added to the reaction tube.The reaction tube was reacted at 140 C for 3 hours, and the reaction product was dissolved in dichloromethane.The product was analyzed by GC/MS (see Figure 5), and the product contained 2-methylbenzofuran.4-methylbenzofuran and 7-methylbenzofuran,There are also benzofuran (obtained from furan itself) and 2,7-dimethylbenzofuran (obtained by self-reaction of 2-methylbenzofuran). Quantitative analysis using GC-FID,The yield of 2-methylbenzofuran was 2.7%, and the yield of 4-methylbenzofuran was 1.9%.The yield of 7-methylbenzofuran was 2.8%.The aqueous acetic acid solution and the main product can be separated and recovered by distillation.
 

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