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[ CAS No. 17092-92-1 ] {[proInfo.proName]}

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Chemical Structure| 17092-92-1
Chemical Structure| 17092-92-1
Structure of 17092-92-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 17092-92-1 ]

CAS No. :17092-92-1 MDL No. :MFCD20926295
Formula : C11H16O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 180.24 Pubchem ID :-
Synonyms :

Safety of [ 17092-92-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P233-P260-P261-P264-P270-P271-P280-P301+P312-P302+P352-P304-P304+P340-P305+P351+P338-P312-P321-P330-P332+P313-P337+P313-P340-P362-P403-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H302-H315-H319-H332-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 17092-92-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17092-92-1 ]

[ 17092-92-1 ] Synthesis Path-Downstream   1~23

  • 1
  • [ 53537-93-2 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
95% With thionyl chloride In pyridine Ambient temperature;
  • 2
  • (-)-methyl azafrinate [ No CAS ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
With nickel(IV) oxide; titanium tetrachloride multistep reaction; 1.) ether/benzene, 5 min, 2.) ether/benzene, RT, 20 h; configuration of the parent compound;
  • 3
  • (3aS,7aR)-2-oxo-3-phenylselenyl-4,4,7a-trimethyloctahydrobenzofuran [ No CAS ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
With dihydrogen peroxide; sodium hydrogencarbonate; acetic acid; platinum 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min; Yield given. Multistep reaction;
  • 4
  • [ 199727-72-5 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
82% With dmap; trifluoromethanesulfonic acid anhydride In dichloromethane 1.) 0 deg C, 1 h, 2.) room temperature, overnight;
  • 6
  • [ 41169-33-9 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 90 percent / 2,2'-isopropylidenebis<(4S)-4-tert-butyl-2-oxazoline>Cu(SbF6)2 / CH2Cl2 / 18 h / Ambient temperature 2: 1.) KOH, 2.) HCl / multistep reaction, 1.) water, ethanol, room temperature, 6 h, 2.) water, room temperature, 12 h 3: 95 percent / hydrogen / (Ph3P)3RhCl / benzene / 12 h / 760 Torr / Ambient temperature 4: 82 percent / trifluoromethanesulfonic anhydride, 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 1.) 0 deg C, 1 h, 2.) room temperature, overnight
  • 7
  • [ 199727-74-7 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 95 percent / hydrogen / (Ph3P)3RhCl / benzene / 12 h / 760 Torr / Ambient temperature 2: 82 percent / trifluoromethanesulfonic anhydride, 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 1.) 0 deg C, 1 h, 2.) room temperature, overnight
  • 8
  • [ 199727-73-6 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 1.) KOH, 2.) HCl / multistep reaction, 1.) water, ethanol, room temperature, 6 h, 2.) water, room temperature, 12 h 2: 95 percent / hydrogen / (Ph3P)3RhCl / benzene / 12 h / 760 Torr / Ambient temperature 3: 82 percent / trifluoromethanesulfonic anhydride, 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 1.) 0 deg C, 1 h, 2.) room temperature, overnight
  • 9
  • [ 104266-24-2 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 81 percent / N,N-dimethylaminopyridine / triethylamine 2: 70 percent / lithium diisopropylamide / -78 °C 3: 95 percent / thionyl chloride / pyridine / Ambient temperature
  • 10
  • [ 104266-25-3 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 70 percent / lithium diisopropylamide / -78 °C 2: 95 percent / thionyl chloride / pyridine / Ambient temperature
  • 11
  • [ 104266-23-1 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: citric acid / methanol / Ambient temperature 2: 81 percent / N,N-dimethylaminopyridine / triethylamine 3: 70 percent / lithium diisopropylamide / -78 °C 4: 95 percent / thionyl chloride / pyridine / Ambient temperature
  • 12
  • (1'RS,3'S)-2',2'-dimethyl-6'-methylene-3'-tetrahydropyranyloxycyclohexylacetic acid [ No CAS ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 7 steps 1: 1.) 0.5 M NaHCO3; 2.) KI, I2 / 1.) ether, r.t., 20 min; 2.) water, reflux, overnight 2: 3.23 g / 0.5percent p-TsOH / methanol / 8 h / Ambient temperature 3: 94 percent / 1.) TfCl, DMAP; 3.) water / CH2Cl2 / 1.) 5 deg C, 10 min; 2.) r.t., 1 h; 3.) 30 min 4: 87 percent / (n-Bu)3SnH / benzene / Ambient temperature 5: 0.960 g / H2 / PtO2 / acetic acid / 23 h / 22800 Torr 6: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 7: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 13
  • ethyl <(1RS,3S)-2,2-dimethyl-6-methylene-3-tetrahydropyranyloxycyclohexyl>acetate [ No CAS ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 8 steps 1: 10.6 g / 2.5percent KOH / ethanol / 2 h / Heating 2: 1.) 0.5 M NaHCO3; 2.) KI, I2 / 1.) ether, r.t., 20 min; 2.) water, reflux, overnight 3: 3.23 g / 0.5percent p-TsOH / methanol / 8 h / Ambient temperature 4: 94 percent / 1.) TfCl, DMAP; 3.) water / CH2Cl2 / 1.) 5 deg C, 10 min; 2.) r.t., 1 h; 3.) 30 min 5: 87 percent / (n-Bu)3SnH / benzene / Ambient temperature 6: 0.960 g / H2 / PtO2 / acetic acid / 23 h / 22800 Torr 7: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 8: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 14
  • (3aRS,5S,7aRS)-4,4-dimethyl-7a-iodomethyl-2-oxo-3-tetrahydropyranyloxyoctahydrobenzofuran [ No CAS ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 6 steps 1: 3.23 g / 0.5percent p-TsOH / methanol / 8 h / Ambient temperature 2: 94 percent / 1.) TfCl, DMAP; 3.) water / CH2Cl2 / 1.) 5 deg C, 10 min; 2.) r.t., 1 h; 3.) 30 min 3: 87 percent / (n-Bu)3SnH / benzene / Ambient temperature 4: 0.960 g / H2 / PtO2 / acetic acid / 23 h / 22800 Torr 5: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 6: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 15
  • [ 104527-56-2 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 2: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 16
  • [ 104527-55-1 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 0.960 g / H2 / PtO2 / acetic acid / 23 h / 22800 Torr 2: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 3: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 17
  • [ 104467-80-3 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 87 percent / (n-Bu)3SnH / benzene / Ambient temperature 2: 0.960 g / H2 / PtO2 / acetic acid / 23 h / 22800 Torr 3: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 4: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 18
  • [ 104435-28-1 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 5 steps 1: 94 percent / 1.) TfCl, DMAP; 3.) water / CH2Cl2 / 1.) 5 deg C, 10 min; 2.) r.t., 1 h; 3.) 30 min 2: 87 percent / (n-Bu)3SnH / benzene / Ambient temperature 3: 0.960 g / H2 / PtO2 / acetic acid / 23 h / 22800 Torr 4: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 5: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 19
  • [ 104435-19-0 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 9 steps 1: 96 percent / 6 h / 140 °C 2: 10.6 g / 2.5percent KOH / ethanol / 2 h / Heating 3: 1.) 0.5 M NaHCO3; 2.) KI, I2 / 1.) ether, r.t., 20 min; 2.) water, reflux, overnight 4: 3.23 g / 0.5percent p-TsOH / methanol / 8 h / Ambient temperature 5: 94 percent / 1.) TfCl, DMAP; 3.) water / CH2Cl2 / 1.) 5 deg C, 10 min; 2.) r.t., 1 h; 3.) 30 min 6: 87 percent / (n-Bu)3SnH / benzene / Ambient temperature 7: 0.960 g / H2 / PtO2 / acetic acid / 23 h / 22800 Torr 8: 1.) LDA; 2.) HMPA / 1.) THF, -70 deg C, 30 min; 2.) THF, allowed to warm to r.t. 9: 1.) 35percent H2O2, AcOH; 2.) NaHCO3, Pt-black / 1.) THF, 5 deg C, 1 h; 2.) r.t., 30 min
  • 20
  • [ 1638-05-7 ]
  • [ 17092-92-1 ]
  • [ 79-77-6 ]
  • [ 432-25-7 ]
  • [ 36340-49-5 ]
YieldReaction ConditionsOperation in experiment
With dihydrogen peroxide; sodium acetate In water at 27℃; for 1h; Enzymatic reaction;
  • 21
  • [ 7235-40-7 ]
  • [ 17092-92-1 ]
  • [ 7500-42-7 ]
  • [ 79-77-6 ]
  • [ 432-25-7 ]
  • [ 36340-49-5 ]
YieldReaction ConditionsOperation in experiment
With dihydrogen peroxide; sodium acetate In water at 27℃; for 1h; Enzymatic reaction;
  • 22
  • [ 1107-26-2 ]
  • [ 17092-92-1 ]
  • [ 7500-42-7 ]
  • [ 79-77-6 ]
  • [ 432-25-7 ]
  • [ 36340-49-5 ]
YieldReaction ConditionsOperation in experiment
With dihydrogen peroxide; sodium acetate In water at 27℃; for 1h; Enzymatic reaction;
  • 23
  • [ 7235-40-7 ]
  • [ 17092-92-1 ]
YieldReaction ConditionsOperation in experiment
With 1H-imidazole; tert.-butylhydroperoxide; mu-carbido bis(2,3,7,8,12,13,17,18-octapropyl-5,10,15,20-tetraazaporphinato)iron(IV); In benzene; at 25℃;Kinetics; The degradation of beta carotene (CCar=(1.64-8.05)10-4 M) was conductedin the presence of 1 (C1=1.610-6 M) and tBuOOH (CtBuOOH =2.7310-2 M) in benzene solution at 25 C. The experiments were controlledspectrophotometrically by decrease in the intensity of absorptionband of carotene at 462 nm. It should be noted that UV-visspectrum of <strong>[7235-40-7]beta-carotene</strong> remains unchanged in pure benzene. In thepresence of tBuOOH for 5 h the intensity of absorption bands onlyslightly decreased and the conversion of beta carotene was limited to ?5%(Table 1). There were no changes observed when 1 was added tobeta carotene benzene solution. When beta carotene, tBuOOH and 1 were simultaneously placed in solution, the disappearance of the beta caroteneabsorption band occurred within 4 min designating that the 1-tBuOOHsystem mediates the process.
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