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CAS No. : | 172899-78-4 | MDL No. : | MFCD08275105 |
Formula : | C9H7NO5 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | N/A |
M.W : | 209.16 | Pubchem ID : | 10846077 |
Synonyms : |
|
TPSA :Topological Polar Surface Area | - | H-Bond Acceptor Count : | - |
XLogP3 : | - | H-Bond Donor Count : | - |
SP3 : | - | Rotatable Bond Count : | - |
Signal Word: | Warning | Class | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
0.22 g (49%) | With hydroxylamine hydrochloride; In ethanol; | A mixture of <strong>[172899-78-4]methyl 3-formyl-5-nitrobenzoate</strong> (0.418 g, 2.0 mmol), hydroxylamine hydrochloride (0.209 g, 3.0 mmol) in ethanol (5.0 mL) was heated at reflux for 2 h. On cooling, the mixture was poured into water and the precipitate collected by filtration. The cake was recrystallized from ethyl acetate-hexane and dried to give 0.22 g (49%) of methyl 3-[(N-hydroxylimino)methyl]-5-nitrobenzoate as an off-white solid, mp 144-145 C. Analysis: Calculated for C9 H9 N2 O5: C, 48.22; H, 3.60; N, 12.50 Found: C, 48.22; H, 3.61;N, 12.41 |
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