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[ CAS No. 180858-08-6 ] {[proInfo.proName]}

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Product Details of [ 180858-08-6 ]

CAS No. :180858-08-6 MDL No. :MFCD28405005
Formula : C10H19NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :WFPAIHVCLZLRLP-UHFFFAOYSA-N
M.W : 217.26 Pubchem ID :90845760
Synonyms :

Safety of [ 180858-08-6 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P270-P301+P312-P330-P501 UN#:
Hazard Statements:H302 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 180858-08-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 180858-08-6 ]

[ 180858-08-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 180858-08-6 ]
  • [ 51534-77-1 ]
YieldReaction ConditionsOperation in experiment
With diisobutylaluminium hydride In tetrahydrofuran; toluene at -78℃; for 1h; F-684.F-684-2 F-684-2 tert-Butyl 4-oxo-butanoate F-684-2 tert-Butyl 4-oxo-butanoate (3276) (3277) N-Methoxy-N-methyl-succinamic acid tert-butyl ester (10.0 g, equivalent to 39.9 mmol) and THF (100 mL) were mixed. Diisobutylaluminium hydride (1.0 M in toluene) (52 mL) was added dropwise to the mixture at -78° C. The mixture was stirred for 1 hr at -78° C. Saturated ammonium chloride was added dropwise to the reaction mixture at ice temperature. To the mixture was added diethyl ether and water. The organic layer was separated, and washed with aqueous saturated ammonium chloride and brine in this order. The organic layer was dried over magnesium sulfate. The magnesium sulfate was filtered off, and the organic layer was concentrated under reduced pressure until being reduced to approximately 60 mL in volume. The resulting the solution was directly used in the next step.
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