[ CAS No. 2489-86-3 ]

Name: 2489-86-3|1-Allylnaphthalene|97%
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SKU: A241419
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COA NMR CNMR HPLC LC-MS

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Product Details of [ 2489-86-3 ]

CAS No. :	2489-86-3	MDL No. :	MFCD00021581
Formula :	C₁₃H₁₂	Boiling Point :	266°C at 760 mmHg
Linear Structure Formula :	-	InChI Key :	-
M.W :	168.23 g/mol	Pubchem ID :	17217
Synonyms :

Safety of [ 2489-86-3 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H302-H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 2489-86-3 ]

Downstream synthetic route of [ 2489-86-3 ]

[ 2489-86-3 ] Synthesis Path-Downstream 1~26

1
[ 2489-86-3 ]
[ 532-31-0 ]
1,2-bis-benzoyloxy-3-[1]naphthyl-propane [ No CAS ]

Reference： [1]Acta Chemica Scandinavica (1947),1950,vol. 4,p. 692,699

2
[ 2489-86-3 ]
[ 86-87-3 ]
[ 120727-51-7 ]

Reference： [1]Journal of the American Chemical Society,1933,vol. 55,p. 2974

3
[ 2489-86-3 ]
[ 37489-99-9 ]

Reference： [1]Chemische Berichte,1951,vol. 84,p. 458,460

4
[ 2489-86-3 ]
[ 22767-77-7 ]

Reference： [1]Journal of the American Chemical Society,1938,vol. 60,p. 1658,1663
[2]Zhurnal Obshchei Khimii,1940,vol. 10,p. 913,915
Chemisches Zentralblatt,1940,vol. 111,p. 3025
[3]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1908,vol. 147,p. 679

5
[ 2489-86-3 ]
[ 217-37-8 ]

Reference： [1]Patent: US2349781,1941,

6
[ 2489-86-3 ]
[ 2765-18-6 ]

Yield	Reaction Conditions	Operation in experiment
96%	With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20℃; under 760.051 Torr; for 12h;	A mixture of <strong>[2489-86-3]1-allylnaphthalene</strong> (16, 33.65 g, 0.2 mol) and 10% Pd/C (1.70 g) was subjected to standard hydrogenation condition at room temperature and atmospheric pressure(balloon). The reaction typically took 12 h to complete. On completion, the reaction mixture was filtered off and the filtrate was evaporated on a rotary evaporator to give a residue, which was purified by column chromatography to yield 2c as a colorless oil (32.69 g, 96%). 1H NMR (DMSO-d6, 400 MHz) : 8.04 (d, 1H, J = 8.0 Hz), 7.87-7.90 (m, 1H),7.74 (d, 1H, J = 8.0 Hz), 7.46-7.53 (m, 2H), 7.40 (t, 1H, J =7.6 Hz), 7.31 (d, 1H, J = 6.8 Hz), 2.98 (t, 2H, J = 7.6 Hz),1.62-1.72 (m, 2H), 0.94 (t, 3H, J = 7.4 Hz). The 1H NMRdata were in good agreement with those reported [20].

Reference： [1]Medicinal Chemistry,2017,vol. 13,p. 260 - 281
[2]Zhurnal Obshchei Khimii,1940,vol. 10,p. 913,915
Chemisches Zentralblatt,1940,vol. 111,p. 3025
[3]Chemische Berichte,1949,vol. 82,p. 161,170
[4]Journal of the Institute of Petroleum,1948,vol. 34,p. 677,680
Chem.Abstr.,1949,p. 2608
[5]Journal of Organic Chemistry,1963,vol. 28,p. 2044 - 2049

7
[ 2489-86-3 ]
[ 27653-17-4 ]

Reference： [1]Journal of the American Chemical Society,1943,vol. 65,p. 1329,1331

8
[ 2489-86-3 ]
[ 120727-51-7 ]

Reference： [1]Acta Chemica Scandinavica (1947),1950,vol. 4,p. 703,706

9
[ 2489-86-3 ]
1-(2,3-dibromopropyl)naphthalene [ No CAS ]

Reference： [1]Organic Letters,2015,vol. 17,p. 2594 - 2597
[2]Zhurnal Obshchei Khimii,1940,vol. 10,p. 913,915
Chemisches Zentralblatt,1940,vol. 111,p. 3025
[3]Organic and Biomolecular Chemistry,2018,vol. 16,p. 9354 - 9358

10
[ 106-95-6 ]
[ 703-55-9 ]
[ 2489-86-3 ]

Reference： [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1908,vol. 147,p. 678
[2]Journal of Fluorine Chemistry,2006,vol. 127,p. 720 - 729

11
[ 107-05-1 ]
[ 703-55-9 ]
[ 2489-86-3 ]

Reference： [1]Zhurnal Obshchei Khimii,1940,vol. 10,p. 913,915
Chemisches Zentralblatt,1940,vol. 111,p. 3025

12
[ 90-11-9 ]
[ 106-95-6 ]
[ 2489-86-3 ]

Reference： [1]Angewandte Chemie - International Edition,2000,vol. 39,p. 2481 - 2483
[2]Chemical Communications,2018,vol. 54,p. 1877 - 1880
[3]Journal of Medicinal Chemistry,1991,vol. 34,p. 2638 - 2643
[4]Bulletin of the Chemical Society of Japan,1979,vol. 52,p. 3632 - 3637
[5]Journal of Organic Chemistry,1963,vol. 28,p. 2044 - 2049
[6]Journal of the American Chemical Society,2008,vol. 130,p. 12901 - 12903
[7]Chemical Communications,2017,vol. 54,p. 66 - 69

13
[ 776-76-1 ]
[ 2489-86-3 ]
[ 22767-77-7 ]
[ 78431-70-6 ]

Reference： [1]Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1981,vol. 30,p. 318 - 321
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1981,p. 401 - 404

14
[ 2489-86-3 ]
[ 1001-48-5 ]
[ 78431-71-7 ]

Reference： [1]Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1981,vol. 30,p. 318 - 321
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1981,p. 401 - 404

15
[ 2489-86-3 ]
[ 68884-32-2 ]

Reference： [1]Journal of Medicinal Chemistry,1991,vol. 34,p. 2638 - 2643
[2]Organic Letters,2015,vol. 17,p. 3346 - 3349

16
[ 91-20-3 ]
[ 106-42-3 ]
[ 107-18-6 ]
[ 2489-86-3 ]
[ 42918-26-3 ]
[ 2489-87-4 ]

Reference： [1]Journal of Organic Chemistry USSR (English Translation),1982,vol. 18,p. 305 - 307
Zhurnal Organicheskoi Khimii,1982,vol. 18,p. 352 - 355

17
[ 112176-15-5 ]
[ 106-95-6 ]
[ 2489-86-3 ]

Reference： [1]Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1987,vol. 36,p. 350 - 355
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1987,p. 391 - 396

18
[ 2489-86-3 ]
[ 106-95-6 ]
[ 63779-65-7 ]

Reference： [1]Journal of the American Chemical Society,1977,vol. 99,p. 4417 - 4424

19
[ 2489-86-3 ]
[ 106-95-6 ]
[ 63779-62-4 ]

Reference： [1]Journal of the American Chemical Society,1977,vol. 99,p. 4417 - 4424

20
[ 2489-86-3 ]
3-(1-naphthyl)-2-chloropropylphosphonic dichloride [ No CAS ]

Reference： [1]Russian Journal of General Chemistry,1995,vol. 65,p. 356 - 360
Zhurnal Obshchei Khimii,1995,vol. 65,p. 406 - 411

21
[ 2489-86-3 ]
[ 31125-58-3 ]
[ 184166-24-3 ]

Reference： [1]Journal of Organic Chemistry,1996,vol. 61,p. 8604 - 8609

22
[ 90-14-2 ]
Allyl-tris-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl)-stannane [ No CAS ]
[ 2489-86-3 ]

Reference： [1]Journal of Organic Chemistry,1997,vol. 62,p. 5583 - 5587

23
[ 90-14-2 ]
[ 106-95-6 ]
[ 2489-86-3 ]

Reference： [1]Angewandte Chemie - International Edition,2000,vol. 39,p. 2481 - 2483
[2]Organic Letters,2001,vol. 3,p. 3201 - 3204
[3]Chemistry - An Asian Journal,2011,vol. 6,p. 2147 - 2157
[4]Organic Letters,2005,vol. 7,p. 4745 - 4747
[5]Angewandte Chemie - International Edition,1998,vol. 37,p. 1701 - 1703

24
polyethylene [ No CAS ]
[ 644-08-6 ]
[ 2489-86-3 ]
[ 83-32-9 ]
[ 208-96-8 ]

Reference： [1]Chemosphere,1999,vol. 39,p. 1497 - 1512

26
[ 2489-86-3 ]
aluminium oxide [ No CAS ]
[ 22767-77-7 ]

Reference： [1]Journal of the American Chemical Society,1938,vol. 60,p. 1658,1663
[2]Zhurnal Obshchei Khimii,1940,vol. 10,p. 913,915
Chemisches Zentralblatt,1940,vol. 111,p. 3025

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P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
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H250	Catches fire spontaneously if exposed to air
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H260	In contact with water releases flammable gases which may ignite spontaneously
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H315	Causes skin irritation
H316	Causes mild skin irritation
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H330	Fatal if inhaled
H331	Toxic if inhaled
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H336	May cause drowsiness or dizziness
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H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 2489-86-3 ]

Quality Control of [ 2489-86-3 ]

Related Doc. of [ 2489-86-3 ]

Product Details of [ 2489-86-3 ]

Safety of [ 2489-86-3 ]

Application In Synthesis of [ 2489-86-3 ]

[ 2489-86-3 ] Synthesis Path-Downstream 1~26

Precautionary Statements-General

Prevention

Response

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Disposal

Physical hazards

Health hazards

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