630-580-1088 sales@ambeed.com
Structure Search

List Search MOL Search Structure Search

0
Chemistry
Asymmetric Synthesis >>Chiral Building BlocksChiral Catalysts, Chiral Ligands and Chiral ReagentsChiral Resolution ReagentsCatalysis Chemistry >>Achiral Crown LigandsC-H ActivationCarbon-Donor LigandsChiral Crown LigandsCross-CouplingCross-Coupling Using Transition Metal CatalystsDACH or Trost LigandsDiketone LigandsHydrogenationChemical Biology >>Conjugation ChemistryGlycoscienceLinkers and CrosslinkersNucleic Acid ChemistryPEGylation
Peptide ChemistryPhotolabile Protecting GroupHeterocyclic Building Blocks >>Acridinium SeriesAliphatic HeterocyclesAromatic HeterocyclesAzetidinesBenzimidazolesBenzisoxazolesBenzodioxansBenzofuransBenzothiazolesInorganic reagents >>Inorganic reagentOrganic Building Blocks >>Acyl ChloridesAlcoholsAldehydesAliphatic Chain HydrocarbonsAliphatic Cyclic Hydrocarbons
AlkenylsAlkylsAlkynylsAmidesOrganometallic Reagents >>Grignard ReagentsOrganoarsenicOrganobismuthOrganoboronOrganogermaniumOrganolithiumOrganomercuryOrganosiliconOrganotinSpecialty Synthesis >>Enzyme-Mediated SynthesisFluorous SynthesisIonic LiquidsSolid Supported SynthesisStains and Dyes >>
Acid DyesAzoic DyesBasic DyesDirect DyesDisperse DyesDye IntermediatesMordant DyesOil DyesOther Stains and DyesSynthetic Reagents >>Acids and BasesC-C Bond FormationC-X Bond Formation (Halogen)C-X Bond Formation (Non-Halogen)Chelation and Complexation CompoundsCondensation AgentsCouplingDehydrating ReagentsFluorination Reagents
Pharmaceutical Intermediates
Analgesics >>BenzhydrocodoneBicifadineCapsaicinCelecoxibDebio-0827DexamethasoneElagolix SodiumEsketamine HydrochlorideIbuprofen sodiumAnesthetics >>CiprofolEsketamine HydrochlorideFospropofol Fospropofol DisodiumLevobupivacaine RemimazolamRemimazolam BesilateRemimazolam besylateRopivacaineAnti-Addiction Agents >>Kakonein
Lofexidine HydrochlorideVarenicline Anti-inflammatory Agents >>ApremilastAsunaprevirATB-346 RelatedBalsalazide BaricitinibBencycloquidium BromideBudesonideCefiderocol Sulfate TosylateCeftaroline Fosamil AcetateAntibacterials >>AFN-1252 RelatedAlatrofloxacin Bedaquiline FumarateBesifloxacin BrilacidinCaspofungin AcetateCefiderocol Sulfate TosylateCefilavancinCeftaroline Fosamil
Anticonvulsants >>BrivaracetamCannabidiolEscitalopram OxalateEslicarbazepine Acetate RelatedFosphenytoinGabapentin EnacarbilJNJ-10234094LacosamideLevetiracetam RelatedAntidementia Agents >>Azeliragon RelatedDavunetideDonepezil HydrochlorideDonepezil RelatedEnsaculinFlorbetaben Flortaucipir F 18Flutemetamol IdalopirdineAntidepressants >>4-Chlorokynurenine
AgomelatineAgomelatine RelatedAllopregnanolone RelatedAmibegronAmitifadineAripiprazole RelatedBasimglurantBefloxatoneAntiemetics >>AprepitantAprepitant RelatedDolasetron RelatedDolasetron Mesylate HydrateFosaprepitant DimeglumineFosaprepitant RelatedOlanzapinePalonosetron RelatedPalonosetron HydrochlorideAntifungals >>Anidulafungin RelatedCabotegravirMore >>
Inhibitors/Agonists
ADCs >>ADC LinkerADC Linker with PayloadAnti-infection >>AntibacterialAntifungalAntiparasiticCCRCMVDengue VirusFilovirusHBVHCVApoptosis >>Apoptosis InducerBcl-2c-Mycc-RETCaspaseDAPKFASG-quadruplex
IAPAutophagy >>CXCRLRRK2MLKOther AutophagysSPHKULKBiochemical Reagent >>Intermediate and OthersBiochemical Reagents >>Biochemical Assay ReagentBiochemicals and Reagents(for Research and Experimental Use)Dye ReagentIntermidate and OthersCell Cycle >>ADC ToxinAPCAurora Kinasec-MycCasein KinaseCDK
ChkCRM1DHFRCytoskeleton >>AktArp2/3 ComplexBcr-AblDynaminFAKGap Junction ProteinHSPIntegrinKinesinDNA Damage >>ATM/ATRDNA Alkylator/CrosslinkerDNA-PKDNA/RNA SynthesisHDACMTH1PARPMore >>
Material Science
Aggregation-Induced Emission >>Other AIE BlocksTetraphenylethylene SeriesElectronic Materials >>Battery MaterialsDye-Sensitized Solar Cell (DSSC) MaterialsElectronic MaterialLiquid Crystal (LC) MaterialsMolecular ConductorsOrganic Light-Emitting Diode (OLED) MaterialsOrganic Solar Cell (OPV) MaterialsOrganic Transistor (OFET) MaterialsPerovskite Solar Cell (PSC) MaterialsMagnetic Materials >>Magnetic Ionic LiquidsMagnetic MaterialMagnetic Metal Complexes Organic Radicals Material Building Blocks >>Ligands for Functional Metal ComplexesLiquid Crystal (LC) Building BlocksPhthalocyanine Building BlocksPolymer and Macromolecule Semiconductor Building BlocksSmall Molecule Semiconductor Building BlocksSolubility Enhancing Reagents
Supramolecular Host Materials Nanomaterials >>Carbon NanomaterialsCeramic MembranesDendrimersGold NanoparticlesIron Oxide NanoparticlesMaterials by ApplicationMesoporous MaterialsMetals and Metal AlloysNano Minerals: NanoclaysOptical Materials >>Coumarin DyesCyanine and Squarylium DyesDCM DyesDipyrromethene DyesFluorescence MaterialsFluorescent ProbesHeat and Pressure Sensitive DyesNear-Infrared (NIR) DyesOrganic Non-Linear Optical (NLO) MaterialsOrganic ligands for MOF materials >>Carboxylic MOF ligandsHalogen seriesMOF ligands of nitrogenous carboxylic acids
Nitrogen containing MOF ligandsOrganic frame monomer blockOther MOF ligandsPorphyrin seriesTwo dimensional MOF ligandsOrganic monomer of COF >>Aldehyde based COF monomerAlkynyl COF monomerAmino COF monomerBoric acid COF monomerCyano COF monomerMultifunctional COF monomerOther COF monomerTriphene seriesOrganic Pigments >>Organic PigmentOther Materials >>Mateial OtherPolymer Science >>MonomersPolymer AdditivesPolymerization ReagentsPolymersResins
Life Science
ADC-linkers >>ADC-linkerAmino Acids >>Amino AcidAmino Acid DerivativesAnalytical Science >>Stable IsotopesAPIs >>API
DNA/RNA >>Nucleosides and NucleotidesEnzymes >>EnzymeOther Life Science >>CRISPR/Cas9eIFIRE1Neuronal Signaling
Sigma ReceptorPeptides >>PeptideStandard Substrates >>Standard SubstrateSteroids >>Other Steroids
Contact Us
Home Cart 0 Sign in  
Chemistry
Heterocyclic Building Blocks
Piperidines
1,1-Dimethyl-4-oxopiperidin-1-ium iodide
Chemistry
Heterocyclic Building Blocks
Organic Building Blocks
Piperidines
Ketones

[ CAS No. 26822-37-7 ]

{[proInfo.proName]} ,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 26822-37-7
Chemical Structure| 26822-37-7
Structure of 26822-37-7 *Storage: {[proInfo.prStorage]}

Search after Editing

*Storage: {[proInfo.prStorage]}

For Research Only 60,000+Inventories Competitive Price 1-2 days Fast Delivery

Quality Control of [ 26822-37-7 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 26822-37-7 ]

SDS

Product Details of [ 26822-37-7 ]

CAS No. :26822-37-7MDL No. :MFCD00466081
Formula : C7H14INO Boiling Point : -
Linear Structure Formula :-InChI Key :-
M.W :255.10Pubchem ID :11149497
Synonyms :

Computed Properties of [ 26822-37-7 ]

TPSA : 17.1 H-Bond Acceptor Count : 2
XLogP3 : - H-Bond Donor Count : 0
SP3 : 0.86 Rotatable Bond Count : 0

Safety of [ 26822-37-7 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P305+P351+P338UN#:N/A
Hazard Statements:H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 26822-37-7 ]

  • Upstream synthesis route of [ 26822-37-7 ]

[ 26822-37-7 ] Synthesis Path-Upstream   1~7

  • 1
  • [ 1445-73-4 ]
  • [ 74-88-4 ]
  • [ 26822-37-7 ]
YieldReaction ConditionsOperation in experiment
88% at 0 - 20℃; for 1.00 h; Step 1: Preparation of 1,1-dimethyl-4-oxopiperidinium iodide [Show Image] Methyl iodide (1.6 mL, 26.5 mmol) was added into a solution of 1-methyl-piperidin-4-one (2.0 g, 17.6 mmol) in acetone (10 mL) at 0 °C. The reaction mixture was stirred at room temperature for 1 hour. The precipitate was filtered off and washed with acetone to afford the title compound as an off-white solid (4.0 g, 88 percent). 1H NMR (D2O, 400 MHz): δ 3.38 (t, J=5.8 Hz, 4H), 3.06 (s, 6H), 1.95-2.05 (m, 4H). LCMS (Method D): Mass found (M+ 128.2), Rt (min): 1.19, Area (percent): 95.3 (Max. Chrom.)
88% at 0 - 20℃; for 1.00 h; Step 1: Preparation of 1,1-dimethyl-4-oxopiperidinium iodideMethyl iodide (1.6 mL, 26.5 mmol) was added into a solution of 1-methyl-piperidin-4-one (2.0 g, 17.6 mmol) in acetone (10 mL) at 0 °C. The reaction mixture was stirred at room temperature for 1 hour. The precipitate was filtered off and washed with acetone to afford the title compound as an off-white solid (4.0 g, 88 percent). 1H NMR (D20, 400 MHz): δ 3.38 (t, J=5.8 Hz, 4H), 3.06 (s, 6H), 1.95-2.05 (m, 4H). LCMS (Method D): Mass found (M+ 128.2), Rt (min): 1.19, Area (percent): 95.3 (Max. Chrom.)
Reference： [1] Journal of Organic Chemistry, 2006, vol. 71, # 22, p. 8602 - 8609
[2] Journal of Organic Chemistry, 2014, vol. 79, # 8, p. 3358 - 3373
[3] Organic Process Research and Development, 2004, vol. 8, # 6, p. 939 - 941
[4] Angewandte Chemie - International Edition, 2008, vol. 47, # 32, p. 5968 - 5972
[5] Journal of the American Chemical Society, 2009, vol. 131, # 1, p. 357 - 367
[6] Patent: EP2508526, 2012, A1. Location in patent: Page/Page column 45
[7] Patent: WO2012/130915, 2012, A1. Location in patent: Page/Page column 55
[8] Journal of Organic Chemistry, 1945, vol. 10, p. 277,278
[9] Journal of the American Chemical Society, 1949, vol. 71, p. 465
[10] Journal of the Chemical Society, 1949, p. 708,712
[11] Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984, # 10, p. 1647 - 1652
[12] Patent: WO2005/90333, 2005, A1. Location in patent: Page/Page column 135
[13] Patent: CN105985355, 2016, A. Location in patent: Paragraph 0692; 0693; 0694; 0695
  • 2
  • [ 1445-73-4 ]
  • [ 108-20-3 ]
  • [ 74-88-4 ]
  • [ 26822-37-7 ]
Reference： [1] Patent: US6884868, 2005, B1
  • 3
  • [ 1445-73-4 ]
  • [ 74-88-4 ]
  • [ 26822-37-7 ]
  • [ 26822-30-0 ]
Reference： [1] Journal of Organic Chemistry, 2005, vol. 70, # 5, p. 1930 - 1933
  • 4
  • [ 41661-47-6 ]
  • [ 26822-37-7 ]
Reference： [1] Patent: CN105985355, 2016, A
  • 5
  • [ 13221-89-1 ]
  • [ 26822-37-7 ]
Reference： [1] Journal of Organic Chemistry, 1945, vol. 10, p. 277,278
  • 6
  • [ 105-71-5 ]
  • [ 26822-37-7 ]
Reference： [1] Journal of Organic Chemistry, 1945, vol. 10, p. 277,278
  • 7
  • [ 25012-72-0 ]
  • [ 26822-37-7 ]
Reference： [1] Journal of the Chemical Society, 1949, p. 708,712

Tags: 26822-37-7 synthesis path| 26822-37-7 SDS| 26822-37-7 COA| 26822-37-7 purity| 26822-37-7 application| 26822-37-7 NMR| 26822-37-7 COA| 26822-37-7 structure

Related Products
Historical Records