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[ CAS No. 279262-88-3 ]

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Chemical Structure| 279262-88-3
Chemical Structure| 279262-88-3
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Product Details of [ 279262-88-3 ]

CAS No. :279262-88-3 MDL No. :MFCD06659872
Formula : C10H15BO3 Boiling Point : 345.492°C at 760 mmHg
Linear Structure Formula :- InChI Key :-
M.W :194.04 g/mol Pubchem ID :-
Synonyms :

Safety of [ 279262-88-3 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 279262-88-3 ]

  • Downstream synthetic route of [ 279262-88-3 ]

[ 279262-88-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 5419-55-6 ]
  • [ 279262-88-3 ]
YieldReaction ConditionsOperation in experiment
53% Stage #1: (4-bromo-2-methyl-phenyl)-propyl ether With n-butyllithium In tetrahydrofuran at -78℃; for 0.333333h; Stage #2: Triisopropyl borate In tetrahydrofuran at -78 - 20℃; for 18.25h; Stage #3: With hydrogenchloride; water 18.2 Step 2; To a solution of 4.7 gm (0.02 mol) of 4-bromo-2 methyl-1-propoxybenzene in 60 mL of dry THF at -78° C. was added 10.6 mL of 2.5 M (0.026 mol) n-BuLi over a 5 min period. The solution stirred at -78° C. for 0.25 hr and 6.1 mL (0.026 mol) of triisopropyl borate was added dropwise. The solution stirred at -78° C. for 0.25 h and allowed to warm to room temperature and continue to stir for 18 hr. The solvent was removed at reduced pressure and 10 mL of conc. HCl was added dropwise. The solid was filtered and triturated with hexanes to yield 2.1 gm (53%) of a white solid that was utilized without further purification and characterization.
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