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[ CAS No. 30335-67-2 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 30335-67-2
Chemical Structure| 30335-67-2
Structure of 30335-67-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 30335-67-2 ]

CAS No. :30335-67-2 MDL No. :MFCD25962062
Formula : C8H4BrNO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :242.03 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 30335-67-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 30335-67-2 ]

[ 30335-67-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2510-03-4 ]
  • [ 30335-67-2 ]
  • 6-amino-10-bromo-12,13-dihydrophenanthro[2,1-b]benzofuran-5-carbonitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
91% With cetyltrimethylammonim bromide; caesium carbonate In water at 20℃; for 24h; 4.2. General procedure for the synthesis of compounds 3, 5, 7, 9 General procedure: To a solution of 1 or 4 or 6 or 8 (0.12 mmol) and 2 (0.10 mmol) in H2O (1 mL) was added Cs2CO3 (32.5 mg, 0.10 mmol) and CTAB(2.0 mg, 5 mol%). The mixture was further stirred at room temperature for the indicated time. Once starting material was consumed (monitored by TLC), the mixture was filtered and the residue was purified by column chromatography on silica gel (petroleum ether/ethyl acetate 8:1 to 3:1) to afford the corresponding product.
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