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[ CAS No. 303780-52-1 ]

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2D
Chemical Structure| 303780-52-1
Chemical Structure| 303780-52-1
Structure of 303780-52-1 *Storage: {[proInfo.prStorage]}

Quality Control of [ 303780-52-1 ]

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Alternatived Products of [ 303780-52-1 ]

Product Details of [ 303780-52-1 ]

CAS No. :303780-52-1MDL No. :MFCD07363817
Formula : C13H14N2O2S Boiling Point : 484.1°C at 760 mmHg
Linear Structure Formula :-InChI Key :-
M.W :262.33Pubchem ID :-
Synonyms :

Computed Properties of [ 303780-52-1 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 303780-52-1 ]

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Application In Synthesis of [ 303780-52-1 ]

  • Downstream synthetic route of [ 303780-52-1 ]

[ 303780-52-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 98-18-0 ]
  • [ 100-51-6 ]
  • [ 303780-52-1 ]
YieldReaction ConditionsOperation in experiment
83% With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; caesium carbonate; In tert-Amyl alcohol; at 120℃; for 12h;Inert atmosphere; Schlenk technique; Under nitrogen, 3-aminobenzenesulfonamide (172 mg, 1 mmol), [Cp * IrCl2] 2 (8 mg, 0.01 mmol, 1Molpercent), cesium carbonate (65 mg, 0.2 mmol), benzyl alcohol (130 mg, 1.2 mmol), t-amyl alcohol (1.0 mL)Were added to a 25 mL Schlenk reaction flask in turn. The mixture was allowed to react at 120 ° C for 12 hours and then cooled to roomThe solvent was removed under vacuum and vacuum. And then purified by column chromatography (developing solvent: ethyl acetate / n-hexane)The target compound, yield: 83percent.
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