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[ CAS No. 3160-59-6 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 3160-59-6
Chemical Structure| 3160-59-6
Structure of 3160-59-6 *Storage: {[proInfo.prStorage]}

Quality Control of [ 3160-59-6 ]

Related Doc. of [ 3160-59-6 ]

SDS

Product Details of [ 3160-59-6 ]

CAS No. :3160-59-6MDL No. :MFCD00027064
Formula : C14H19NO4 Boiling Point : 442.8°C at 760 mmHg
Linear Structure Formula :-InChI Key :N/A
M.W :265.31Pubchem ID :2724772
Synonyms :

Computed Properties of [ 3160-59-6 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 3160-59-6 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P301+P312-P302+P352-P304+P340-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 3160-59-6 ]

  • Downstream synthetic route of [ 3160-59-6 ]

[ 3160-59-6 ] Synthesis Path-Downstream   1~10

  • 1
  • [ 3160-59-6 ]
  • (2S,3S)-2-(N-chloramino-N-benzyloxycarbonyl)-3-methylpentanoic acid [ No CAS ]
  • 2
  • [ 110-91-8 ]
  • [ 3160-59-6 ]
  • [(1S,2S)-2-Methyl-1-(morpholine-4-carbonyl)-butyl]-carbamic acid benzyl ester [ No CAS ]
  • 3
  • [ 3160-59-6 ]
  • [ 540508-49-4 ]
  • [ 540508-28-9 ]
  • 4
  • [ 3160-59-6 ]
  • [ 540508-43-8 ]
  • (2S,3R)-3-{4-[2-((2S,3S)-2-Benzyloxycarbonylamino-3-methyl-pentanoylamino)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-phenoxy}-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester [ No CAS ]
  • 5
  • [ 3160-59-6 ]
  • [ 1668-10-6 ]
  • [ 49762-53-0 ]
  • 6
  • [ 3160-59-6 ]
  • [ 403790-74-9 ]
  • [(2S,3S)-2-((2S,3S)-2-Benzyloxycarbonylamino-3-methyl-pentanoylamino)-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-acetic acid tert-butyl ester [ No CAS ]
  • 7
  • [ 3160-59-6 ]
  • [ 351442-24-5 ]
  • [ 351442-33-6 ]
  • 8
  • [ 3160-59-6 ]
  • [ 293732-23-7 ]
  • [ 293732-61-3 ]
  • 9
  • [ 3160-59-6 ]
  • [ 293732-53-3 ]
  • [ 293732-39-5 ]
  • 10
  • [ 2783-17-7 ]
  • [ 3160-59-6 ]
  • [ 201004-33-3 ]
YieldReaction ConditionsOperation in experiment
81% To a solution of 42.98 g (0.162 mol) of N-benzyloxycarbonyl-L-isoleucine in 150 mL of ethyl acetate was added 36.73 g (0.178mol) of N,N'-dicyclohexylcarbodiimide at 0 C. After the mixture was stirred for 1 h at 0 C, a solution of 16.22 g (0.081 mol) of 1,12-dodecamethylenediamine in 150 mL of chloroform was added, and this solution was stirred for 2 h at 0 C for a further 2 h at room temperature. The resulting mixture was stirred for 10 h at 40 C and then at 55 C overnight. After removing the formed dicyclohexylurea by hot filtration, the filtrate was cooled to room temperature and the gel formed was suction filtered and dried. The crude product was dissolved in 1.2 L of hot 1-propanol and cooled to room temperature. The gel formed was broken well using a mechanical stirrer and suction filtered. After repeating this purification with 1-propanol, 45.48 g (81%) of the dodecamethylenediamide of N-benzyloxycarbonyl-L-isoleucine was obtained.
Historical Records

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[ 3160-59-6 ]

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(2R,3R)-2-(((Benzyloxy)carbonyl)amino)-3-methylpentanoic acid

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