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Chemistry
Organic Building Blocks
Benzene Compounds
Cbz-L-Isoleucine
Chemistry
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Organic Building Blocks
Amino Acids
Benzene Compounds
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[ CAS No. 3160-59-6 ]

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Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 3160-59-6
Chemical Structure| 3160-59-6
Structure of 3160-59-6 *Storage: {[proInfo.prStorage]}

Search after Editing

*Storage: {[proInfo.prStorage]}

For Research Only 60,000+Inventories Competitive Price 1-2 days Fast Delivery

Quality Control of [ 3160-59-6 ]

COA GC NMR CNMR HPLC LC-MS

Related Doc. of [ 3160-59-6 ]

SDS

Product Details of [ 3160-59-6 ]

CAS No. :3160-59-6MDL No. :MFCD00027064
Formula : C14H19NO4 Boiling Point : 442.8°C at 760 mmHg
Linear Structure Formula :-InChI Key :N/A
M.W :265.31Pubchem ID :2724772
Synonyms :

Computed Properties of [ 3160-59-6 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 3160-59-6 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P301+P312-P302+P352-P304+P340-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 3160-59-6 ]

  • Downstream synthetic route of [ 3160-59-6 ]

[ 3160-59-6 ] Synthesis Path-Downstream   1~10

  • 1
  • [ 3160-59-6 ]
  • (2S,3S)-2-(N-chloramino-N-benzyloxycarbonyl)-3-methylpentanoic acid [ No CAS ]
Reference： [1]Synlett,2005,p. 223 - 226
  • 2
  • [ 110-91-8 ]
  • [ 3160-59-6 ]
  • [(1S,2S)-2-Methyl-1-(morpholine-4-carbonyl)-butyl]-carbamic acid benzyl ester [ No CAS ]
Reference： [1]Journal of Organic Chemistry,2003,vol. 68,p. 7505 - 7508
  • 3
  • [ 3160-59-6 ]
  • [ 540508-49-4 ]
  • [ 540508-28-9 ]
Reference： [1]Tetrahedron Letters,2003,vol. 44,p. 2557 - 2560
  • 4
  • [ 3160-59-6 ]
  • [ 540508-43-8 ]
  • (2S,3R)-3-{4-[2-((2S,3S)-2-Benzyloxycarbonylamino-3-methyl-pentanoylamino)-1-(tert-butyl-dimethyl-silanyloxy)-ethyl]-phenoxy}-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester [ No CAS ]
Reference： [1]Tetrahedron Letters,2003,vol. 44,p. 2557 - 2560
  • 5
  • [ 3160-59-6 ]
  • [ 1668-10-6 ]
  • [ 49762-53-0 ]
Reference： [1]Journal of the American Chemical Society,2001,vol. 123,p. 9935 - 9946
  • 6
  • [ 3160-59-6 ]
  • [ 403790-74-9 ]
  • [(2S,3S)-2-((2S,3S)-2-Benzyloxycarbonylamino-3-methyl-pentanoylamino)-3-(tert-butyl-dimethyl-silanyloxy)-butyrylamino]-acetic acid tert-butyl ester [ No CAS ]
Reference： [1]Tetrahedron Letters,2001,vol. 42,p. 8955 - 8957
  • 7
  • [ 3160-59-6 ]
  • [ 351442-24-5 ]
  • [ 351442-33-6 ]
Reference： [1]Organic letters,2001,vol. 3,p. 2061 - 2064
  • 8
  • [ 3160-59-6 ]
  • [ 293732-23-7 ]
  • [ 293732-61-3 ]
Reference： [1]Chemical and Pharmaceutical Bulletin,2000,vol. 48,p. 920 - 934
  • 9
  • [ 3160-59-6 ]
  • [ 293732-53-3 ]
  • [ 293732-39-5 ]
Reference： [1]Chemical and Pharmaceutical Bulletin,2000,vol. 48,p. 920 - 934
  • 10
  • [ 2783-17-7 ]
  • [ 3160-59-6 ]
  • [ 201004-33-3 ]
YieldReaction ConditionsOperation in experiment
81% To a solution of 42.98 g (0.162 mol) of N-benzyloxycarbonyl-L-isoleucine in 150 mL of ethyl acetate was added 36.73 g (0.178mol) of N,N'-dicyclohexylcarbodiimide at 0 C. After the mixture was stirred for 1 h at 0 C, a solution of 16.22 g (0.081 mol) of 1,12-dodecamethylenediamine in 150 mL of chloroform was added, and this solution was stirred for 2 h at 0 C for a further 2 h at room temperature. The resulting mixture was stirred for 10 h at 40 C and then at 55 C overnight. After removing the formed dicyclohexylurea by hot filtration, the filtrate was cooled to room temperature and the gel formed was suction filtered and dried. The crude product was dissolved in 1.2 L of hot 1-propanol and cooled to room temperature. The gel formed was broken well using a mechanical stirrer and suction filtered. After repeating this purification with 1-propanol, 45.48 g (81%) of the dodecamethylenediamide of N-benzyloxycarbonyl-L-isoleucine was obtained.
Reference： [1]Chemical and Pharmaceutical Bulletin,2000,vol. 48,p. 920 - 934
[2]Bulletin of the Chemical Society of Japan,2018,vol. 91,p. 1176 - 1185

Tags: 3160-59-6 synthesis path| 3160-59-6 SDS| 3160-59-6 COA| 3160-59-6 purity| 3160-59-6 application| 3160-59-6 NMR| 3160-59-6 COA| 3160-59-6 structure

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Similar Product of
[ 3160-59-6 ]

Chemical Structure| 28862-89-7

A223186[ 28862-89-7 ]

(2R,3R)-2-(((Benzyloxy)carbonyl)amino)-3-methylpentanoic acid

Reason: Optical isomers