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[ CAS No. 35288-49-4 ] {[proInfo.proName]}

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Chemical Structure| 35288-49-4
Chemical Structure| 35288-49-4
Structure of 35288-49-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 35288-49-4 ]

CAS No. :35288-49-4 MDL No. :MFCD01109676
Formula : C12H8Cl2O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 255.10 Pubchem ID :-
Synonyms :

Safety of [ 35288-49-4 ]

Signal Word:Danger Class:8
Precautionary Statements:P264-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P362+P364-P403+P233-P501 UN#:3261
Hazard Statements:H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 35288-49-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 35288-49-4 ]

[ 35288-49-4 ] Synthesis Path-Downstream   1~5

  • 2
  • [ 1675-54-3 ]
  • [ 35288-49-4 ]
  • polymer; monomer(s): 2,2-bis[4-(2,3-epoxypropoxy)phenyl]propane; p-phenylene diacryloyl chloride [ No CAS ]
YieldReaction ConditionsOperation in experiment
64% With tetrabutylammomium bromide In toluene at 100℃; for 12h;
  • 4
  • [ 35288-49-4 ]
  • [ 19417-59-5 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: Heating 2: H2 / Pd/C / tetrahydrofuran / 40 - 50 °C 3: LiAlH4 / tetrahydrofuran / 50 - 60 °C 4: HBr / 120 - 130 °C
  • 5
  • [ 6052-73-9 ]
  • [ 35288-49-4 ]
  • C22H20N2O4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% To the solution of 5,6-dihydropyridine-2(1H)one (64.1 mg, 0.66 mmol, 2.2 equiv) in THF (3.0 mE, 0.1 M) at-78C. was added solution of n-BuLi in hexanes (413 tL, 1.6 M, 0.66 mmol, 2.2 equiv) and stirred for 15 minutes. To this solution was added 1 ,4-phenylenediacryloyl chloride (77 mg, 0.30 mmol) and the reaction was stirred at -78C. for 3 hours. Reaction mixture was diluted with ethyl acetate, quenched with aqueous ammonium chloride, extracted with EtOAc, washed with brine, dried with anhydrous sodium sulfate and purified by column chromatography using hexanes-ethyl acetate gradient (0 to 80% EtOAc), yielding 81.3 mg of the product (72%).
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